GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\28324A.D Vial: 3 Acq On : 5 Feb 2002 12:22 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Acetic acid, 3-[1,3]dioxola... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.92 0.26 ug/L 167003 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 2 3 -(CYCLOHEX-3'-EN-YL)PROPANOL $$ . . . 174 C8H14O4 015745-87-6 36 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 9 Abundance Scan 223 (5.920 min): 28324A.D (-) m/z 73.10 100.00% 7)3

5000 43 TII 87 103 5.60 5.80 6.00 6.20 57 0- ■ ■ i ■1111 ‘'11111' ''r 1111'11’, '11 m 1 ThmmmuuPTTT m/z 43.10 23.92% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

AAAA 5000- ‘' I ‘ ' I ' ' ' ' I1 1 1 1 1 1 1 ' 1 I 5.60 5.80 6.00 6.20 43 m/z 45.10 8.78% 27 55 , 87 113 174 0- '11'1 " i''1' r TTI 11'' " i " 11, 1i ' 1" i " 111" rrP1111''''1111111" " i ■ ■ ■111 r'11" " i' " 111 m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 1 1 1 | 1 1 1 1 | 1 1 * ' 1 1 1 1 1 1 1 1 ’ 1 1 5.60 5.80 6.00 6.20 5000 m/z 41.10 6.84% 43 27 55 , i , 87 113 174 r TTI 111 I " 1 'T 1 1 1 I 1 1 11 I 1 1 ITI ' । । ' | i'l । 1 | . 1 , , । , T-r| i I I I | I i i i | I I । । । i | I I | i 0- " r " ' i' miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... — 30 5.60 5.80 6.00 6.20 73 m/ z 71.10 5.69% 5000 44 58

15 ... /.......... n/z-> 0 H .................. i " ' ■ i '1 " i " ' ■ ir " ' i'1111 ■ " ' i'1'' i' " ‘ i'1 " i " 111' ■ " 11 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 11 ' ' I ' ' ' ' I 1 1 1 1 I 1 1 1 ' I 1 ' ’ 1 I 5.60 5.80 6.00 6.20

’8324A.D SCAN508.M Fri Feb 22 11:44:12 2002 Page 5

NYC-WTC_000004866

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