GCMS analysis results for sample AE01637, March 2002

Machine-extracted title · confidence 100%

GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010106–000010125

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report . Data File: C: \MSDCHEM\1\5973N\02FEB21\01637.D Vial: 6 Acq On : 21 Feb 2002 7:22 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.95 0.36 ug/L 168054 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 38 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ ... 174 C8H14O4 015745-87-6 38 3 N-Ethylformamide $$ N-Formylethy. . . 73 C3H7NO 000627-45-2 9 4 1-Hexanol, 6-amino- 117 C6H15NO 004048-33-3 9 Abundance Scan 228 (5.948 min): 01637.D (-) m/z 73.10 100.00% 73

5000 43 — ■ ■ I ‘ 1 ‘ • i ■ ■ ■ ■ i ‘ ' ‘^'1 r . ■ . । .

5.60 5.80 6.00 6.20 1155...,■ 87 01* 11 ■ 11 < 11 > ■ 11 • . .. ] 1. . . |. . . . j . . . ‘14 I.. i.' i'. ।।1।।।।।।।. m/z 43.10 25.56% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 — AA 5.60 5.80 6.00 6.20 M ‘I’IA

43 m/z 41.10 9.48% 27 0- “ i ■ ■ ■ ■ i ■" ■ i • TTmm ,I '. | . .87 113 174 . 55 . r. | | . I .'I. ' !. . . . | > . ' . | . ' . . | . .. . | . . . . | . I ' . | . niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3’-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 5.80 6.00 6.20 " 1 ' 5000- m/z 45.10 9.15% 43 27 55 , । ■I, .. ।..87 113 174 0- i', ।......... । .-i.. ।.... ।.... ।.... ।.... ।.... ।. 11111 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... ■ ' i 1 1 ■ ■ i ■ ■ • ■ i ■ • ■ ■ i ■ 30 5.60 5.806.00 6.20 73 m/z 71.00 7.21%

5000 44 58

15 0- 118)4 [l .. ।.।.... ।.... (.... ।.... (.... ।.... ।.... ।.... ।. • ■ i ■ 1 ■ • i • ‘ ■ i 1 ■ ■ ■ i ■ ■ ■ ■ i 1 m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

01637.D HP022102.M Mon Feb 25 10:55:44 2002 Page 8

NYC-WTC_000010117

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NYC-WTC_000010117Source: NYC Law Department, mirrored locally

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GCMS analysis report for sample AE01636, March 2002 · Box DEP Box 14

NYC-WTC_000010086

GCMS laboratory results for sample AE01636 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998