GCMS analysis results for sample AE02720, March 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report • .Data File : C:\MSDCHEM\l\5973N\02FEB28\02720.D Vial: 5 Acq On : 28 Feb 2002 6:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Acetic acid, 3-[1,3]dioxola... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.94 0.38 ug/L 160391 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 33 3 N-Ethylformamide $$ N-Formylethy. . . 73 C3H7NO 000627-45-2 9 4 Pentanol, 5-amino-__________________ 103 C5H13NO 002508-29-4 9 Abundance Scan 227 (5.936 min): 02720.D(-) m/z 73.10 100.00% 73

5000 43 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i 1 ■ ■ ■ i ‘ ■ i 5.60 5.80 6.00 6.20 41.58— ,i, 87 103 m/ z 43.10 27.00%

N_ 0- i1 • “ i ■ • • ■ i . . ■ । I l . . । . I I . ( . .. , । . । . . . . ।. , . . । , . . . । . . . . t . J , ! . . . i | i i . I | i niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 NA ■ 1 i ■ ■ • ■ i ■ 5.60 5.80 6.00 6.20 43 m/z 41.10 11.34% 0- "i'•" i ‘ ■11" 27 mHpm , , 55 1" i" 111"1 ■ I"' ■ i I 87 113 " i1 ■' ■ i1 ■ ■ ■ i" ■ ■ i1 “ ■ i • ■ ■ ■ i •' ■' i ■ 174 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 5^80 6.00 6.20 5000 m/ z 45.10 9.68% 43 27 , 87 —mm0-0113 174 0- p 55 , । Tumnt1 —umo!u—Rap miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 5.60 5.80 6.00 6.20 ' ‘ 73 m/z 71.10 6.99% 5000 44 58

15 - 0- — 11 ' ‘ I ‘ ‘ ‘ 1 I ' 1 ' 11 1 ‘ ' I 1 ‘ ‘ I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

02720.D HP022102.M Fri Mar 01 10:07:42 2002 Page 6

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