GCMS analysis results for sample AE03075, March 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report • 'Data File : C: \MSDCHEM\1\5973N\02FEB28\02717 . D Vial: 2 Acq On : 28 Feb 2002 3:30 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.94 0.35 ug/L 126559 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 227 (5.936 min): 02717.D (-) m/ z 73.10 100.00% 73

5000 43 ' ' I ' ' ‘ ‘ I ' ' ' ■ I ‘ 11 1 1 1 1 ' I 55 5.60 5.80 6.00 6.20 , ———87 0 - ‘ i *'1' I • ’ ’ * I ‘ 1 103 aUTWDTWILTLTT m/z 43.0.0 24.36% nlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

________ _____________________ A 5000 ‘ ‘ i ' ' ' ' i • ■ 1 ■ i ■ ■ ■ ‘ i ‘ ‘ • i 5.60 5.80 6.00 6.20 43 m/z 41.10 11.46% 27 87 ।.. |'i i ■ 1111'.. ।... 1 , 113 ■ i " ■ ■ i ■" ' i “ ■ ■ i ■ ■■ ■ i 174 . 55 , 0- * i • > • • i * 1 ■' i1 ■1' i ■■ ■■ i ■■ ■■ i “ i ■1 ■■ i ■ miz- > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 ■ • i ' ■ ■ ■ i ■ ■ 1. 1 1 1 ' ■ ' • i 5.60 5.80 6.00 6.20 5000 m/ z 45.00 9.71% 43 27 55 , 87 113 174 0- ‘ 1 ■ • i'i । ■ 11 |‘ 1 ’1+4*’1444 ‘T ■ I ■. I . . I'. I. I ri I n 111 I H I 11 : |Tr> > 11 ri 111 11 11 I ■ 1 I 11 I 111 I niz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9665:3-Pentanol, 3-methyl- 1 ' I ■ ■ ■ ' i ■ • ■ ■ 1 • 1 ■ ■ i * ■ ■ ■ i 73 5.60 5.80 6.00 6.20 m/z 71.00 6.45% 5000 55 45 87 27 m/z—> O-TT —H 20 30 40 -' " I ‘ 50 60 70 80 | ।।.i । ■ i ■ । i i ■ i । 11 i i 11 i > i |-m r | i i i i 11 > i . । > ■ 90 100 110 120 130 140 150 160 170 180 1 ' i ■ • ■ ■ f ■ ' ■• i ■ ■ ■ ' i ' ' ■ ■ i 5.60 5.80 6.00 6.20

02717.D HP022102.M Fri Mar 01 10:07:21 2002 Page 7

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