GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\00003A.D Vial: 2 Acq On 5 Feb 2002 3:46 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Acetic acid, 3-[1,3]dioxola... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.92 0.25 ug/L 188979 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 3 Pentanol, 5-amino- 103 C5H13NO 002508-29-4 9 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 223 (5.920 min): 00003A.D (-) m/z 73.10 100.00% 73

5000 43 1 ■ t > 1 ' 1 J 1 11 * I 1 1 1 ' I , 87 103 5.60 5.80 6.00 6.20 I 1 । fl ′′ 0V m 11 rIn 57 1111’ " " r r ’ " i■ i " " i " " i " " I'1" i "'' i " ■1 r ''' i ‘ m/ z 43.10 26.33%

J. iz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 4K 5.60 5.80 6.00 6.20 43 m/z 45.10 10.40% 27 55 87 113 174 0- — 11 ■'111''1 'T‘ Pp T ‘i TTT r 11 ■ i' " 11 Tl/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 AA5.60 5.80 MA, ' r1 1 1 1 'i 6.00 6.20 5000 m/ z 41.10 9.44% 43 27 55 87 113 174 0- tin......'I1'1' 11 ■ ■'11 “ 1 ’I’ । " I ■ i I " " I " 111" I " " I i1" ■ i ■ i ■1 ■ ■ i ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance 33 #9904: Pentanol, 5-amino- AAAMAA ■ ' 11 ‘■ ■ 1 i1 1 ■ 1 i'1 1 1 i1 1 1 1 i 5.60 5.80 6.00 6.20 m/z 71.10 6.13% 5000

n/z-> , 43 56 0^ ■ I ' ■ ■ ■ i1111 ■ i • ilii . । 20 30 40 50 60 67 85 103 111 < > । > 11, । ■ > ।, । < i < > 11 > > > 11 > > 11 > >, 11 < ।' 11 > 111 > < < 11 < 11. । <

70 80 90 100 110 120 130 140 150 160 170 180 5.60 A... 5.80 6.00 6.20

00003A.D SCAN508.M Thu Feb 21 10:18:50 2002 Page 7

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