GCMS analysis results for sample AE00832, Feb 4 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00832.D Vial: 5 Acq On : 31 Jan 2002 1:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetic acid, 3-[1,3]dioxola... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.92 0.48 ug/L 260772 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3’-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H14O 000994-05-8 33 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 223 (5.920 min): 00832.D (-) m/z 73.10 100.00% 70

5000

43 5.60' 1 ' i ' ' ■ ■ 1 1 r ‘‘ 1 I

I I 55 1.. 87.. 103........................ 5.80 600 6.20 o ■ । ■ 111 p - m/z 43.10 22.39% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70

5000 AN).. 5.60 5.80 6.00 6.20 43 m/z 45.10 10.13%

n/z-> 27 01TT 20 30 40 — P 50 60 70 87 113 1" ।1 *OuuBunnummOIT 174 Ti 1 ' 1T 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 M\ n 1 1 1 I1 1 * * | ' r pT 1* pi rr i | 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.29% 43 27 55 , 87 113 174 o1TTTIIT TTTT TTTTTTr ' " p ■11 r ‘ ' p 1 ■' i11 ■ ■ p '11 p'' ■ i ■' ‘' i1111 r ‘11 p 1' ■ 11 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... —AAA—A A AM 11 111 1 ■ 1 ■ i 70 5.60 5.80 6.00 6.20 m/z 74.10 5.13% 5000

55 87 27 45 0 ' r 1'111 ‘ " i11" iI TTTT 11 ■'11111 ■ ■ i1 ■' ■ i1 ■' ■ i " 1 ■ i I' ■1 ■ 111111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00832.D SCAN508.M Fri Feb 01 09:18:51 2002 Page 3

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