GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report - Data File : C:\MSDCHEM\1\5973N\02FEB05\00004A.D Vial: 3 Acq On 5 Feb 2002 4:36 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Acetic acid, 3-[1,3]dioxola... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.92 0.21 ug/L 170099 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 42 23-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 42 3 Pentane, 3-methoxy- $$ 1-Ethylpr. .. 102 C6H14O 036839-67-5 25 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 223 (5.920 min): 00004A.D (-) m/z 73.10 100.00% 73

5000 43 ' ' 1 1 > ■ ' l 1 ■ ■ ■ l

55 5.60 5.80 6.00 6.20 O-PTT mll . II i ■ ■ ‘' i ■ ■1 ■ i' , 87 103 m/z 43.10 27.94% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 w/AgAp ........... 5.60 5.80 6.00 6.20 43 m/z 45.10 10.79% 27 55 113 87 174 0- I '"''I .T" l'!1'1- 11" " 11 “ ' I' • •• i1 Tt 1’***—******’*’**’’**) n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 ............... Al J 5.60 5.80 6.00 6.20 5000 m/z 41.10 10.76% 43 27 87 . 0-TTTTTT ■ ■ ■ i111 ■ । 55 i 11111 ''l1 +TT TITuuun113 174 —uuOuOPTr m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9698: Pentane, 3-methoxy- $$ 1-Ethylpropyl methyl ether AAA N 1 i * ' 1 1 i 73 5.60 5.80 6.00 6.20 m/ Z 71.00 5.80%

5000 45

27 55 - 0 - '1'7151111711111111111'16110B"-133EITT-T--""I1" m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00004A.D HP020702.M Thu Feb 21 15:48:47 2002 Page 6

NYC-WTC_000004829

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