DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB01\31505.D Vial: 6 Acq On : 1 Feb 2002 6:53 pm Operator: Sample : 508 scan fb Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetic acid, 3-[1,3]dioxola... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.92 0.46 ug/L 189538 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 23-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Pentanol, 5-amino- 103 C5H13NO 002508-29-4 9 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 223 (5.920 min): 31505.D (-) m/ z 73.10 100.00% 73

5000 43 ' ' ' i ' 1 1 ‘ i ■ 1 ' ■ I 1 1 ' 1 I ' 1 ' 1 I

55 87 103 5.60 5.80 6.00 6.20 oV 4441 4— m/z 43.10 25.48% m/z-> 20 30 40 50 60 70 80 !90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 A । IM । । । । । । । 5.60 5.80 6.00 6.20 43 m/ z 45.10 9.75% 27 55 87 0- TT PTTT . ................113 —1—0001——0I1——00—174 UTTT miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5.60 5.80 6.00 6.20 5000 m/ z 41.10 8.68% 43 27 55 87 113 174 0-TTTTT74r 'T' 'I "i "I'' i'1 '' l1'1' 11111 111 " 111'11'1 trl’r"’ 11। 111111 n/z- > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9904: Pentanol, 5-amino- ' ' T ' ■ ■ ‘ 1 1 1 1 1 I 33 5.60 5.80 6.00 6.20 m/ z 71.10 8.47%

5000

n/z—> OTTT 20 -43567 —*—0--- 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

31505.D SCAN508.M Mon Feb 04 10:14:21 2002 Page 3

NYC-WTC_000004134