DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02FEB27\02385.D Vial: 1 Acq On : 27 Feb 2002 3:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 8 Acetic acid, 3-[1,3]dioxola... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.94 0.40 ug/L 182786 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 2 3- (CYCLOHEX-3'-EN-YL)PROPANOL $$ . . . 174 C8H14O4 015745-87-6 36 3 Pentanol, 5-amino- 103 C5H13NO 002508-29-4 9 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 227 (5.936 min): 02385.D (-) m/ z 73.10 100.00% 73

5000-

43 ■ ■ i > ■ • ■ i ■ ■ ■ ■ । । । । 5,60 5.80 6.00 6.20 nlz—> 01. ।.... । ■ 20 30 4 80 90 100 110 120 130 140 150 160 170 180 40 50 60 70 1.87.... 103....................................... m/z 43.10 23.88% Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 AAA 5.605.80 6.00 6.20 1 ■ i ' ■ 1 1 i

43 m/ z 41.10 9.05% 27 113 174 55 0-- 11111111" 111 . i , 87 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 A Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 1 1 1 5.80 6.00 AAA 6.20 5000 m/ z 45.10 8.34% 43 27 55 , 87 113 174 01 ' 111''' I''11 ‘I’M 1‘ ‘141‘11 'T' 11m—u—uwPm—mumIOOTOO]T n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance 33 #9904: Pentanol, 5-amino- ---A-44 5.60 5.80 6.00 6.20 m/z 71.0.0 6.62% 5000

, 0^ 11—00’0———/————]————] 43 56 67 85 1 03 ■ ■ i ' ■ ■ ■ i m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

32385.D HP022102.M Thu Feb 28 08:47:03 2002 Page 10

NYC-WTC_000005019