GCMS analysis results for sample AE01507, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

.' Data File : C:\MSDCHEM\l\5973N\02FEB21\01506 .D Vial: 3 Acq On : 21 Feb 2002 12:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Acetic acid, 3-[1,3]dioxola... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.95 0.44 ug/L 185010 1,4-Dichiorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 228 (5.948 min): 01506.D (-) m/z 73.10 100.00% 73

5000 43 1 . I k . . . 1 1 . . . 1 . . IPg ‘ ■ I' 5.60 5.80 6.00 6.20 miz-> O-PTT 20 30 —40l , 87 103 11' i"i11" r'1111"111" " i11 “ i IT ■ i1' ■ ■ i ‘ 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ■ ■ i ■ ‘' ■ i ■ m/Z 43.10 23.89% Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 • • i ■ 1 1, 5.60 5.80 6.00 6.20 43 m/ z 45.10 10.69% 27 55 87 113 174 0- 4 I ‘1 "I "'‘u i ■ i1 ■ ■ ■ i ■ ■ i “ " i ■ " ' i " *' i ■11 ■ 11 m/z-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 5.80 6.00 6.20 5000 m/ z 41.10 9.92% 43 27 55 87 113 174 01111 ■ 111 +r • i “ " 11 •1114Pp i i'i 11111 |,... । ri।।1।11l ■1 > * i ■ mfc-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9663:3-Pentanol, 3-methyl- 73 5.60 5.80 6.00 6.20 m/z 71.00 7.97%

5000

_ 55 45 27 87 01 ., j 1 . • , i i * “l •,.. • i‘ “ i ‘1 । ■ —p 1 “ 11'''1 0—0 * ■ i • ■ ' * i ■ ■ ■ ■ i ' 1 ■ ■ i • ■ ‘ ■ i ‘ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

01506.D HP022102.M Mon Feb 25 10:54:44 2002 Page 5

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