GCMS blank results for sample AE03508, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03508.D Vial: 4 Acq On : 8 Mar 2002 1:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Acetic acid, 3-[l,3]dioxola... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 3.89 ug/L 1874100 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 3 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6/33 3 N-Ethylformamide $$ N-Formylethy. . . 73 C3H7NO 000627-45-2 9 4 3-Pentanol, 2,4-dimethyl-___________ 116 C7H160 000600-36-2 9 Abundance Scan 223 (5.891 min): 03508.D (-) m/z 73.10 100.00% 70

miz-> 5000

0-

Abundance 10 43

,1, 87 103 .. । TTT.. ।. TT ।।।।111111111111111111 ■ 11 ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #78238: Acetic acid, 3-[1 ,3]dioxolan-2-ylpropyl ester A 5.60 5.80 6.00 6.20 m/z -43.10 25.18% • ■ । ‘ ■

70

500) ■ I 1 1 5.60 5.80 6.00 6.20 43 m/z 45.10 10.02%

L 27 87 0 np 55 ’ ’’111131 ‘ .t p 113 174 ।. i.. ।.., .| ri..!.,. 111111111111 n 11111 >>11h111 miz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3’-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 70 • ‘ I ’ ‘ * 1 11 * 1 11T TIIT 1 1 '' 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.65% 43 27 0- nmppmt| 1’552’11111117Hp 87 113 TTTTrpTTrp-t-rrp- rrrTTT 118T[T 174 ]T TTTTTT TT tt TTT tt miz-> 10 20 3040 50 60 70 80 90100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 • • • i • A — 6.20 5.60 5.80 6.00 —.— 73 m/z 71.00 6.78% 5000 44 58

15 H 0- 1 '1..... 4 — 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 A 1 I I 1 I 1 I ’1 miz-> 5.60 5.80 6.00 6.20

03508.D HP022102.M Fri Mar 15 10:08:51 2002 Page 10

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