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GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02

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Scanned page image, NYC-WTC_000004886
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\29232A.D Vial: 4 Acq On 5 Feb 2002 1:13 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Acetic acid, 3-[1,3]dioxola. .. Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 5.92 0.26 ug/L 197392 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ . .. 174 C8H14O4 015745-87-6 36 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2- (3-bromo-5,5,5-... 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 223 (5.920 min): 29232A.D (-) m/z 73.10 100.00% 73

5000 43 87 103 5.60 5.80 6.00 6.20 0- L...... 111107111/1584111177 —TUUTETTTTT m/z 43.10 22.79% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 A4 V1 1 I 1 1 1 1 I 5.60 5.80 6.00 6.20 43 m/ Z 41.10 8.52% 27 ! [ , 87 113 174 0 mN 55 * I “ ‘ ' I " 1 ‘14T——n1—mm—001/n mz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 5.80 AAAA. 6.20 6.00 5000 m/z 45.10 8.32% 43 27 55 , 87 113 174 0-TTT ' l" " 1" ' 'T, । 1" i " 1' i " " i " " i '* ■' i ■ " ' i " ‘' i " " i " " I " " i'1" i ‘ m/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 5.60 5.80 A.MW., 6.00 6.20 73 m/z 71.00 6.57%

5000 44 58

15 0 v1s1... TWTT]—muuOpTROu n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

29232A.D SCAN508 .M Fri Feb 22 11:44:18 2002 Page 7

NYC-WTC_000004886

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