GCMS analysis results, sample AE02719, March 2002

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Library Search Compound Report • Data File : C: \MSDCHEM\1\5973N\02FEB28\02719.D Vial: 4 Acq On : 28 Feb 2002 5:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.94 0.39 ug/L 138801 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 45 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 45 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 1-Nonanamine 143 C9H21N 000112-20-9 9 Abundance Scan 227 (5.936 min): 02719.D (-) m/z 73.10 100.00% 73

5000' 43 ■ ■ i ■ ■ • ■ i ■ ■ • 1 i 5.60 5.80 6.00 6.20 0- . .................. . . —9mma 10 87 —92*mmBBmmmmnnr m/z 43.10 22.59% niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 A { . A 5000 5.60 5.80 6.00 6.20 43 m/z 41.10 8.47% 27 55 , 87 ,i 1mpa0munatu 113 174 0- mppm TMTIIPT ———7fupmmamDTmatg nz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 A IB T I 5.60 5.80 6.00 6.20 5000 m/z 45.10 7.79% 43 27 55 . , 87 113 174 0- 1 ■ i'1" i “ “ i ■ T •’—00—1—0020011) miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... ' 1 i ' ■ • ' I ■ ■ ’ ■ r1 ' ' ' I ' 1 1 1 I 3b 5.60 5.80 6.00 6.20 73 m/z 71.00 5.37% 5000 44 58

m/z—> 0 m 15 — TTTemum]mmum*ppugnmPPTMT] 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 ■ ' i ■ ■ ■ • i 6.20

02719.D HP022102.M Fri Mar 01 10:07:34 2002 Page 9

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