GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\29232A.D Vial: 4 Acq On 5 Feb 2002 1:13 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 6 2-Propanone, 1,1,1-trichlor... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T. 6.01 0.06 ug/L 41741 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3 36 2 l-Hexadecanol (CAS) $$ Cetal $$ ... 242 C16H340 036653-82-4 9 3 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3 9 4 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3 9 Abundance Scan 231 (6.011 min): 29232A.D (-) m/z 43.10 100.00% 43

5000

, 61 85 । 97 125 -A 5.60 14 111‘+I+*1*I’’ 5.80 6.00 6.20 6.40 0 “ 1 “ 1 ‘ 11] .......... iT...... Il........ 1 “ I' ‘ “ I " ' ■ 1' ‘ ’ 1 1" ' ‘ 1 ‘ ‘ "I >••>!> i11 “ ।>■■' ।■ i ■ ■■ ■ i'" ’ i' ■ ” i ■ ■ ■ ■ । " i" m/z 124.90 13.23% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #59079:2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 43

5000 5.60 5.80 6.00 6.20 6.40 m/z 97.00 12.48% i or 97 125 35 0 '...... I 1... 5. h. 117 1......... 11" “ I'1 111111101107011"1010110101111111111110131111111332103170737791""IBTBTIT-T /z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #177034: 1-Hexadecanol (CAS) $$ Cetal $$ Ethal $$ Ethol $$... 43 55 83 5.60 5.80 6.00 6.20 6.40 5000 70 97 m/z 46.90 9.08% 111 A 125 O-ITT -rp-TT -HHTTITTTTTTTTTTTTTTTTTTTTTTTHTTT 196 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #59078:2-Propanone, 1,1,1 -trichloro- (CAS) $$ Trichloroac... 43 5.60 5.80 6.00 6.20 6.40 m/z 127.00 8.27% 5000

0 Tg ■ i.,ri ■1"61 82 97 117125 35 i1 ■111 ‘11111 IT’ 11 ''i11" I"''' I'1" i ■ ■ ■11 ■ ■" i ■ ■ ■' i" " i' ■ " i ■ ■1 ■ i ■ ■ ■ ■ i' ■ iz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 5.60 5.80 6.00 6.20 6.40

29232A.D SCAN508.M Fri Feb 22 11:44:18 2002 Page 8

NYC-WTC_000004887

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