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GCMS analysis results, sample AE03616, March 2002

Machine-extracted title · confidence 75%

Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.

NYC-WTC_000037780–000037799

Folder label: “GCMS X 2/19/02 A 3/8/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03616.D Vial: 6 Acq On : 8 Mar 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 2-Propanone, 1,1,1-trichlor... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

6.00 0.31 ug/L 193863 1, 4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- $$... 160 C3H3C13O 000918-00-3 6 2 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3/ 0 3 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3 50 4 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C130 000918-00-3 25 Abundance Scan 233 (6.004 min): 03516.D (-) m/z 43.10 100.00% 4)3 1 _

5000

■ i • • ’’11’11 prT-rT-p-r-r-r-j-r-r 97 125 5.60 5.80 6.00 6.20 6.40

m/z-> +4953.... 434 0- I I | I TT i | > I . . | . . Tiif 117 L 10 20 30 40 50 60 70 80 90 100 110 120 130 11 m/z 124.90 10.20% Abundance #59081:2-Propanone, 1,1,1-trichloro- $$ .alpha.,.alpha.... 43

5000- 5.60 5.80 6.00 6.20 6.40 m/z 97.00 6.23% 15 0- ■ ■ । • ■ I • • । ■ ■ ■ ■ । 35 । ■ ,49 85 97 117 125 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59078: 2-Propanone, 1,1,1 -trichloro- (CAS) $$ Trichloroac... 43 > i * • • • i ■ — 1 i ■■ ■ ■ i ■ • 5.60 5.80 6.00 6.20 6.40 5000 m/ z 82.90 5.99%

35 49 61 82 I • I • ■ ■ ■ i • ■ ■ ■ । 117■ i ‘125 ‘ i • > 97 0- ' ‘ i ' *1 ■ i ‘ ■ i ■■ i ■ ■ TT । । ।।. miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59079: 2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 43 5.60 5.80 6.00 6.40 m/z 46.95 5.32% 5000

97 125

m/z—> 35 0- ........... I ■ ' i1 ■ ■ ■ i ■ • • • i • • ■ • i ‘ 10 20 30 40 49 85 117 . IITT-p-r +4... ............. .... ’’II11-741111161 50 60 70 80 90 100 110 120 130 LAAAAAAAAL 5.60 5.80 6.00 6.20 6.40

03516.D HP022102.M Fri Mar 15 10:09:36 2002 Page 10

NYC-WTC_000037793

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NYC-WTC_000037793Source: NYC Law Department, mirrored locally

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