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GCMS analysis results for sample AE03617, March 28, 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.

NYC-WTC_000037800–000037818

Folder label: “GCMS X 2/19/02 A 3/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C :\MSDCHEM\1\5973N\02MAR08\03517.D Vial: 7 Acq On 8 Mar 2002 8:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Propanone, 1,1,1-trichlor... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

6.00 0.34 ug/L 197028 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# 'Qual

1 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3 56 2 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3 15 3 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3/45 4 2-Propanone, 1,1,1-trichloro- $$... 160 C3H3C130 000918-00-3 38 Abundance Scan 233 (6.004 min); 03517.D (-) m/z 43.10 100.00% 43

5000

IIIr 1 • i ■ 1 5.60 580 6.00 6.20 6.40 0- ■ • । ■1 ■ i1 ‘ । 1 , 151 , , 61,....... 83. 97,103 _ 119125 • i1 * ‘ ‘ I ’ • ’ ‘ M ' I ’ ’ ’ ‘ I 111 ‘ | * ’ ’ • ’ * ) 1 * < • I ’ ‘ ‘ 1 J ’ ‘ m/z 124.90 10.16% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59078: 2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 43

5000 5.60 5.80 6.00 6.20 6.40 m/z 47.00 7.13%

miz-> 0^TTTPTeum TT 10 20 30 35 40 49—14. 971t 117 125 ■ i ■ ■ • • i ■ ■ ■ ■ i • • ■ ■ i • ■ ■11 • ■ 50 60 70 80 90 100 110 120 130 Abundance #59079: 2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 43 5.60 5.80 ' ' 6.00 6.20 6.40 5000 m/z 126.90 6.67%

85 97 125 35 49 Jl 0- ‘ ‘ i '' ■ ■ i 1 ' '' i 1 ' ' 1 i'1 •11 * • • • [ • * • * । • — r I J IJ I I I TT 1 * I 1 TTn TT 117 II miz-> 10__ 20 30 40 50 __ 60 70 80 90 100 110 120 130 Abundance #59082: 2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 43 5.60 5.80 6.00 6.20 6.40 m/z 82.90 6.16% 5000

15 27 , 49 63 85 97, 110 117 127 0 ■ ‘ i ■ ‘ I ‘ i ■ ■ • ■ i ■ 1 ■ ‘ i ■ 1 . .'J , , . I TTT TTT—t* TTT TITT TTI I I I I |' I I I1, | I T | r I 1 1 I ' ‘ ■ • l T | । » ' • | > r m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.60 5.80 6.00 6.20 6.40

03517.D HP022102.M Fri Mar 15 10:09:42 2002 Page 11

NYC-WTC_000037814

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NYC-WTC_000037814Source: NYC Law Department, mirrored locally

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