GCMS analysis results for sample AE03617, March 28, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03617.D Vial: 7 Acq On : 8 Mar 2002 8:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Heptane, 2,2,3,4,6,6-hexame. . . Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 8.59 0.09 ug/L 50378 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane, 2,2,3,4,6,6-hexamethyl- 184 C13H28 062108-32-1 50 2 Butane, 2,2,3,3-tetramethyl- $$ ... 114 C8H18 000594-82-1 50 3 Octane, 2,5,6-trimethyl- 156 C11H24 062016-14-2 50 4 Decane, 2,2,7-trimethyl- 184 C13H28 062237-99-4 45 Abundance Scan 462 (8.589 min): 03517.D (-) m/z 57.10 100.00% 57

5000 43 71 A....... — —AA 85 99 8.20 8.40 8.60 8.80 9.00

mz-> 0-PmmH I T M i •■* ■i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 i “ ‘ ■ i ■ ■ ■ ■ i m/z 43.10 37.30% Abundance #93465: Heptane, 2,2,3,4,6,6-hexamethyl- 57

5000 43 AAM— 8.20 8.40 8.60 lalu 8.80 9.00 71 85 m/z 56.10 36.77%

miz-> 0- —.... 2.... .... ' ------13 12- 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #15710: Butane, 2,2,3,3-tetramethyl- $$ Ethane, hexamethyl... 57 - 8.20 8.40 8.60 8.80 9.00 5000 m/z 71.10 20.26% 41

27 ■nfe-> 15 ■ 0-TTCTTIU1 r T 111" ‘ I .,“i 1 +.. 83... *..... ........... 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #56277: Octane, 2,5,6-trimethyl- —r-j-n . , TI88II j ,,,,,, s 57 8.20 8.40 8.60 8.80 9.00 m/z 41.10 19.47%

5000 43

miz-> 85 99 *»j *» L 0 111131 ‘I . t i 11 * t * 11TT______ + 70 127 156 -PH 1,11111111117/117171111111113 10 20 30 40 50 60 70 80 !90 100 110 120 130 140 150 160 8.20 8.40 8.60 8.80 9.00

03517.D HP022102.M Fri Mar 15 10:09:42 2002 Page 12

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