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GCMS blank results for sample AE03510, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.

NYC-WTC_000037680–000037699

Folder label: “GCMS X 2/19/02 A 3/8/02”

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Scanned page image, NYC-WTC_000037693
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03510.D Vial: 6 Acq On : 8 Mar 2002 2:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Decane, 2,5,6-trimethyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 8.59 0.13 ug/L 67094 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual/ 1 Decane, 2,5,6-trimethyl- 184 C13H28 062108-23-0 74 2 Octane, 2,5,6-trimethyl- 156 C11H24 062016-14-2 2 3 Heptane, 2,2,3,4,6,6-hexamethyl- 184 C13H28 062108-32-1/64 4 Heptane, 2,2,4-trimethyl- $$ 2,2... 142 C10H22 014720-74-2 59 Abundance Scan 462 (8.589 min): 03510.D (-) m/ z 57.10 100.00% 57

5000 43 71 85 99 . A8.80A 9.00 4 8.20 8.40 8.60 miz-> 0- ‘i■■‘ ■ i ‘11 ■ 20 30 40 T 50 + • i ■"11 “1 • i > 60 70 80 90 100 110 120 130 140 150 160 m/z 56.00 35.33% Abundance #93445: Decane, 2,5,6-trimethyl- 57 43

5000 ■ i 1 ■ ‘ ■ i 1 ■ 8.20 8.40 A i ■ * ■ • i • ■ • ■ i ■ ■ 8.60 8.80 9.00 71 m/z 43.10 26.80% 84

miz-> Qinmmm 20 30 40 50 - 60 70 80 90 9113 ....... 100 110 120 130 140 150 160 Abundance #57SZ77: Octane, 2,5,6-trimethy-- 57 AAAA AMAnA 8.20 8.40 8.60 8.80 9.00 5000 43 m/z 71.10 23.66%

70 85 +L 0-11′131 pili 118 T rp-n 20 30 40 50 60 70 i TTONT ..... 99.............. 127 80 90 100 1i0 120 130 ........ 156 140 150 160 miz-> Abundance #93465: Heptane, 2,2,3,4,6,6-hexamethyl- A 57 8.20 8.40 8.60 8.80 9.00 m/z 41.10 18.08% 5000 43 71 85

miz—> 0 —2.. r... + 20 30 113 127 TTTmusmouom—utmTgT 60 70 80 90 100 110 120 130 140 150 160 40 50 ' I' ‘'11" 8.20 8.40 M 8.60 • • i ’ 8.80 • * i * * 9.00

03510.D HP022102.M Fri Mar 15 10:09:05 2002 Page 10

NYC-WTC_000037693

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NYC-WTC_000037693Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

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