GCMS blank results for sample AE03614, March 28, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03614.D Vial: 4 Acq On : 8 Mar 2002 6:03 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Octane, 2,5, 6-trimethyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

8.59 0.12 ug/L 57525 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Octane, 2,5,6-trimethyl- 156 C11H24 062016-14-2 59 2 Heptane, 2,2,4-trimethyl- $$ 2,2... 142 C10H22 014720-74-2 50 3 Decane, 2,2,8-trimethyl- 184 C13H28 062238-01-1 42 4 Hexane, 2,2,5-trimethyl- 128 C9H20 003522-94-9 42 Abundance Scan 462 (8.589 min): 03514.D(-) m/z 57.10 100.00% 57

5000 41 71 85 99 A--P 8.20 8.40 — 8.60 —AA 8.80 9.00

miz-> 0- । r PPP ■ i 4 1111J 20 30 40 50 60 — 70l — —- 80 90 100 110 120 130 140 150 160 170 m/z 56.10 34.74% Abundance #56277: Octane, 2,5,6-trimethyl- 57

5000 43 ’ i 1 T-r+TV-n-r-p _A ■ ■ । ■1 8.20 8.40 8.60 8.80 9.00 m/z 41.10 24.65% 70 85 miz-> 0-• I ‘ 20 __ L " I' ‘ ‘'I 11• ‘ I ‘ ' 30 40 ... i.... 4.. 9.......127——.... 156,.... 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #38873: Heptane, 2,2,4-trimethyl- $$ 2,2,4-Trimethylheptane 57 ‘ I ‘ ‘ ' I ‘ ' I A 8.20 8.40 8.60 8.80 9.00 5000 m/z 43.10 22.41% 43 27 71 0- 1 — H -TT 2 miz-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 #93437: Decane, 2,2,8-trimethyl- A 1 i 1 ' TT i • > 57 8.20 8.40 8.60 8.80 9.00 m/z 71.10 20.54%

5000

71 .27 42 85 99 113 127 169 0 TPPp 'I I ""'I1' TPTTTD i" " i ■ '11 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 8.20 8.40 8.60 8.80 9.00

03514.D HP022102.M Fri Mar 15 10:09:24 2002 Page 12

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