GCMS analysis results, sample AE03616, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03616.D Vial: 6 Acq On : 8 Mar 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Decane, 2,5,6-trimethyl- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 8.59 0.09 ug/L 52887 1,4-Diehlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Decane, 2,5,6-trimethyl- 184 C13H28 062108-23-0 74 2 Octane, 2,5,6-trimethyl- 156 C11H24 062016-14-239 3 Heptane, 2,2,3,4,6,6-hexamethyl- 184 C13H28 062108-32-1 39 4 Octane, 2,4,6-trimethyl- 156 C11H24 062016-37-9 38 Abundance Scan 462 (8.589 min): 03516.D (-) m/z 57.10 100.00% 57

5000- 43 71 85 99 2.................. ■ i ■ ■ ■ ■ i ' 1 ■ 8.20 8.40 i 8.60 —AA 8.80 9.00 01 i, 1 1 1 1 1 ‘ III ’ ‘ ‘ I ’ J,...... 1............................ _ m/z 56.00 29.69% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #93445: Decane, 2,5,6-trimethyl- 57 43

5000 ■ i > * • * । 8.20 8.40 ■ ). 1 । • • • • । • • ■ • । ■1 8.60 8.80 9.00 71 84 m/z 43.10 26.40%

mz-> 0-1IIPIIPI + 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 .11 n 113 127 TTIOTTITRTII

Abundance #56277: Octane, 2,5,6-trimethyl- 57 NAAA 8.20 8.40 [‘ 8.60 AAAAA 8.80 9.00 5000 43 m/z 71.10 24.48%

miz-> 0- t | . t n | . i : . (

Abundance 20 30 40 . p : l 50 + 60 70 — 85 99 127 156 ’I- — ■' i • ■ ■ ■ i ■11' I''1' I'1'' P 1111'' 70 80 90 100 110 120 130 140 150 160 #93465: Heptane, 2,2,3,4,6,6-hexamethyl- —• । ■ • ■ • । ‘ । ■ ■ • • ) • ' । । । । 57 8.20 8.40 8.60 8.80 9.00 m/z 41.10 21.15% 5000 43 71 85 ......... , 113 127 O' ‘ J ‘ . ............ ‘ | ‘ T’IIIT I I | I 4 ----- TI—u—n—uputnma*pr m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 8.20 8.40 8.60 8.80 9.00

03516.D HP022102.M Fri Mar 15 10:09:36 2002 Page 11

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