Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
NYC-WTC_000037800–000037818Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
If Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02MAR08\03617 .D Vial: 7 Acq On : 8 Mar 2002 8:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************* * * * ********************* Peak Number 11 N-perdeuteriobenzylideneani ... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 116175 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual l N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64, 2 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 000000-00-0 53 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 /50 4 Pyrazine, tetraethyl- (CAS) $$ t... 192 C12H20N2 038325-19-8 50 Abundance Scan 1675 (22.283 min): 03517.D (-) m/z 192.00 100.00% 102
5000 k 96 146 -160 82 22.00 22.20 22.40 22.60
m/z—> 0 mHTHH 42 52 70 p 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I+ m/z 191.00 21.94% Abundance #88409: N-perdeuteriobenzylideneaniline 192
5000 82 __ l . j < . .T 11T • • i * • 22.00 22.20 22.40 22.60 54 110 m/Z 96.00 16.54%
m/z—> 0- 30 mm 1 ■i•■ ■•i“ 1 94 mM 160 • ■ ■ • I “ “ I “ “ I “ “ I “111‘“1111 “1111 r 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 U Abundance #102788:2,5-Dihydrophosphole, 3-methyI-1-oxo-1-phenyl- 192 164 1 ' 1 ‘ 1 1 1 I ’ 1 • i ■ • 22.00 22.20 22.40 22.60 5000 99 m/z 193.00 16.44% 115 47 77 177
0 —IHIIIpg 11111121111111 1 125134 146 l 4— m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene ‘ ‘ ‘ ‘ ‘ I ‘ ‘ • t • • • ■ • 192 22.00 22.20 22.40 22.60 m/z 146.00 13.12% 5000
miz—> 0- I ” ’11 8.4. 96 139 152 165 176 TIUIBIEEpu“mnhuuufi p1" I “ ’ ‘ I ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ...... 4.... /I 22.00 22.20 22.40 2260
03517.D HP022102.M Fri Mar 15 10:09:42 2002 Page 13
NYC-WTC_000037816
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NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037740
Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037660
Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037700
Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000037604
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
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Reference standard analysis data verifying instrument performance for detecting volatile organic compounds in water samples.
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NYC-WTC_000037616
Laboratory report showing GCMS blank analysis results for volatile organic compounds with detection limits below MDL.
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NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
Filed in the same folder