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← Document results/DEP Box 28/GCMS X 1/11/02 A 1/31/02
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GCMS analysis results for sample AE00833, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00833 including surrogate recovery and unknown compounds.

NYC-WTC_000052069–000052087

Folder label: “GCMS X 1/11/02 A 1/31/02”

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Scanned page image, NYC-WTC_000052084
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00833.D Vial: 1 Acq On : 31 Jan 2002 2:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 N-perdeuteriobenzylideneani ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 130326 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 50 3 1,4-Dimethyl-3,5-propanobicyclo[... 192 C13H20O 000000-00-0 46 4 Phenanthrene, 3-methyl- $$ 3-Met... 192 C15H12 000832-71-3 40 Abundance Scan 1656 (22.280 min): 00833.D (-) m/z 192.10 100.00% 192

5000

82 96 146 160 22.00 22.20 22.40 22.60

/z-> 40 52 66 | 0 " I " " I " " 11' " I'11' I" '111 i pl.... 118 I ■ ■ ............... . t'l. ।' mMmryerpnorr 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I m/z 191.10 19.63% Abundance #88409: N-perdeuteriobenzylideneaniline 102

5000 82 TT 22.00 22.20 22.40 22.60 54 110 m/z 96.00 16.58% 30 I 94 160 0 — rrI’T v -H —opmmtmpmp T-q-n m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192

22.00 22.20 22.40 22.60 5000 m/z 193.10 16.06%

96 ............................................ ................... 139 152 165 176 0 । -l ■ ■ r-ri. . ................................ 'I |' | "" I v m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103601:1,4-Dimethyl-3,5-propanobicyclo[2.2.2]octan-2-one — TT 107 192 22.00 22.20 22.40 22.60 159 m/ z 146.10 13.20% 119 93 5000 132 145 174

m/z--> 0 " i " '' i " '11" ' ■ i ’ ■ " r ■ > ■ i " ■ ■ i ■ " ' r " ■ r ■ " i " " i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 '' I' ‘‘ I" H u ' * i........ I 111 "T r‘ar10f 22.00 22.20 22.40 22.60

00833.D SCAN508.M Fri Feb 01 09:18:59 2002 Page 12

NYC-WTC_000052084

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NYC-WTC_000052084Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

machine-extracted · confidence unavailable · Check page ↗

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