GCMS analysis results for sample AE00833, Feb 2002

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Laboratory report showing GCMS analysis of sample AE00833 including surrogate recovery and unknown compounds.

NYC-WTC_000052069–000052087

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00833.D Vial: 1 Acq On : 31 Jan 2002 2:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.46 ug/L 387952 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 86 2 Acridine-D9 188 C13D9N 000000-00-0 80 3 Phenanthrene-dlO 188 C14D10 001517-22-2 80 4 N-(perdeuteriobenzylidene)-4-deu... 188 C13H4D7N 000538-51-2 64 Abundance Scan 1699 (22.771 min): 00833.D (-) m/z 188.15 100.00% 158

5000

94 Imae* _ 80 22.40 22.60 22.80 23.00 23.20

n/z-> 40 54 66 0 TPTr , । h 1.1,, 111..... -II. | 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ......... 132.,,146. Ma trrmn m/z 189.20 18.25% Abundance #84502: Anthracene-d10- 188

5000 , I , , , r, , r, T-1 r r. , I . I I I I , 22.40 22.60 22.80 23.00 23.20 m/z 94.10 17.51% „ 80 94 160 66 i i 1 1 I " 1 1 I 1 ' PT i । । i । i I । । । । | I I । । | । । > i । .. i i | > i n | i , i i । i 1801 Of 'I""!1'11 T1nnn] n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #85254: Acridine-D9 188 ,1.2 22.40 22.60 22.80 23.00 23.20 5000 m/z 80.10 12.40% fl 93 158 66 80 j| — n/z-> O- r 11 " ' ■ i ’1" i11' ■ i'1' ■ 11'r' i'' ’ ■ r ■1 ■ i " ■' i • ■'' i " '' i 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 188 TI

I "IT ' < 1 । ■ 1 TPBnTT 22.40 22.60 22.80 23.00 23.20 m/z 184.10 10.32%

5000

80 160 66

n/z-> Op ■ l • ■ • ■ l ■' ■ ■ I' • l • l ■ 30 40 50 60 70 I ''1' I ’''' I'1' ' I 80 90 100 110 120 130 140 150 160 170 180 190 — .189... 22.40 22.60 22.80 23.00 23.20

30833.D SCAN508.M Fri Feb 01 09:19:00 2002 Page 13

NYC-WTC_000052085

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NYC-WTC_000052085Source: NYC Law Department, mirrored locally

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