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GCMS analysis results for sample AE00833, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00833 including surrogate recovery and unknown compounds.

NYC-WTC_000052069–000052087

Folder label: “GCMS X 1/11/02 A 1/31/02”

←Page 18 of 19→
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00833.D Vial: 1 Acq On : 31 Jan 2002 2:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L *************************************************************** * * * * * * Peak Number 12 6-methyl-5-(3 4'-methylene... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.

29.68 0.03 ug/L 24566 Chrysene-dl2 30.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 6-methyl-5-(34'-methylenedioxy... 244 C12H12N402 000000-00-0 56 2 3-[2-(2,5-dimethylpyrrol-l-yl)-4... 244 C14H16N2O2 119836-21-4 56 3 Sophoramine 244 C15H20N2O 006882-66-2 56 4 enxo-2-(phenylimino) -3-methyl-1, ... 244 C15H20N2O 105545-43-5 46 Abundance Scan 2304 (29.678 min): 00833. D (-) m/z 244.10 100.00% 244

5000 122 49 84 212 29.40 29.60 29.80 30.00 0 - < । 1 1 । । r1 ' ' IT 1 1 1 1 1 1 I1 m/Z 243.10 63.13% lz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #178493: 6-methyl-5-(3',4'-methylenedioxyphenyl)pyrimidine... 24.4

5000 29.40 29.60 29.80 30.00 m/z 121.90 26.65% 185 . N 0- n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #178978: 3-[2-(2,5-dimethylpyrrol-1 -yl)-4-pyridyl]propioni... 24.4 1 1 1 ' 1 1 r"' 1 ' ' I ' ' ' ' I 1 ' 94 29.40 29.60 29.80 30.00 5000 m/ Z 49.00 20.45% 229

0-TPT m/z->_____ 40 Abundance 60 80 100 120 140 #179289: Sophoramine

136 160 180 183

200 220 240 24.4 N / W / AW

m/z ‘3T 1 1 1 1 ' I' ' I ' ' ' 1 29.40 29.60 29.80 30.00 84.00 i 20.18%

5000 MV 149 215 96 109 122 । 160 172 186 0-TPTPT I. TT— 1 r1 r 1 i 1 1 1 1 i 1’’* ‘ I /z-> 40 60 80 100 120 140 160 180 200 220 240 29.40 29.60 29.80 30.00

00833.D SCAN508.M Fri Feb 01 09:19:00 2002 Page 14

NYC-WTC_000052086

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NYC-WTC_000052086Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

machine-extracted · confidence unavailable · Check page ↗

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