GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB05\30644A.D Vial: 1 Acq On 5 Feb 2002 2:56 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 4-Amino-5,5-dimethyl-2-meth... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

29.69 0.05 ug/L 55231 Chrysene-dl2 30.51

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-Amino-5,5-dimethyl-2-methoxyca... 243 C15H17NO2 118089-29-5 50 10 2 9-Amino-1-phenyl-3,6-diazahomoad... 243 C15H21N3 000000-00-0 50 3 6-methyl-5-(3 4‘-methylenedioxy... 244 C12H12N402 000000-00-0 50 4 1-Pyrenecarboxaldehyde hydrazone 244 C17H12N2 076465-53-7 50 Abundance Scan 2305 (29.690 min): 30644A.D (-) m/z 244.20 100.00% 24.4

5000 122 1 ■ i ■ ' ‘ I‘ 84 108 ...............................198 212 ........... j । 29.40 29.60 29.80 30.00 44 | — Of 'I ..................... ... i 1 m/z 243.10 59.40% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #177722:4-Amino-5,5-dimethyl-2-methoxycarbonyl-3-phenyl-c... 244

5000 ■ ' i ■ ■ ■ ■ i 1 29.40 29.60 29.80 30.00 m/z 122.10 26.66% 167 184 196 212 J 0+ > [ । > > > !’ i 1 ’ । i”) । । । । । । । । । । । । । । । । I . i I । . . r . । . . . . । r m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #177798: 9-Amino-1 -phenyl-3,6-diazahomoadamantane 243 1 1 i ■ 1 1 1 I ■ 1 42 29.40 29.60 29.80 30.00 56 m/z 245.20 18.64% 5000 72 170 156 214 146 184 200 0! ■m1 'I ■ ■ rti-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #178493: 6-methyl-5-(3‘,4‘-methylenedioxypheny!)pyrimidine... 1 ■ i ■ ' ■ ■ i ' 1 ■ i ' ■ ■ ' i ' ' 244 29.40 29.60 29.80 30.00 m/z 242.10 17.63%

5000

185 . 0- , ............... I _ iz—> 40 60 80 100 120 140 160 180 200 220 240 29.40 29.60 29.80 30.00

30644A.D SCAN508.M Fri Feb 22 11:44:25 2002 Page 15

NYC-WTC_000004914

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