Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02721 including surrogate recovery.
NYC-WTC_000011007–000011026Folder label: “GCMS X 2/5/02 A 2/28/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB28\02721 .D Vial: 6 Acq On : 28 Feb 2002 6:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 4-Amino-5,5-dimethyl-2-meth... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 29.69 0.03 ug/L 15726 Chrysene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-Amino-5,5-dimethyl-2-methoxyca. .. 243 C15H17NO2 118089-29-5 5 2 N-(tert-Butyloxycarbonyl)-1-amin... 243 C12H21NO4 000000-00-0 4 3 N-(tert-Butyloxycarbonyl)-1-amin... 243 C12H21NO4 000000-00-0 4 4 11-Hydroxymethyl-4,4,10-trimethy... 243 C11H17NO5 000000-00-0 3 Abundance Scan 2331 (29.688 min): 02721 .D (-) m/z 244.00 100.00% 207 244
5000
29.40 29.60 29.80 30.00 0 ••i>• • j ■ • •• t >* • • । * i * • “ i1 *“ i * * • ■ i * ■ * * i • ri j 11 * 111 w 11 > । > ij 1111 * 11 (11 11 * p-rrrp-rrr m/z 206.90 89.01% m/z-> 160165170175180185190195200 205 210215 220 225230235 240245 250 Abundance #177722:4-Amino-5,5-dimethyl-2-methoxycarbonyI-3-phenyl-c... 244
5000 29.40 29.60 29.80 30.00 m/z 243.00 77.69% ..167... 184.. 196... 212........ 0 . . | . ! . . | . I ■ , ( , . , , I , , . ! | l n I |1 i ! < | . . , . I I . . . | I I I I | ! I 1 I I I | I ! | I | I | | 1 ! I ! | | . I | | l n 1 | ! I ! ! | l ! niz-> 160165170175180185190195 200 205210215220225 230235 240245 250 Abundance #177485: N-(tert-Butyloxycarbonyl)-1-amino-2>2-dimethylcyc... 108
29.40 29.60 29.80 30.00 5000
244 01 • ‘ I ’ “ ’ I “ “ I “ “ I * * “ I ‘“ 1 * ‘ . । ..I. ।..... । ।11■ miz-> 160165170175180185190195200 205210215220225230235240245250 Abundance #177484: N-(tert-ButyloxycarbonyI)-1-amino-trans-2,3-dimet... 188
5000
244 0 1111011—0020000980002277 > ।< 11 > 111111> 11 > I> । > 1111 > । < > > 11 • • 1111.ii-p-nrpiT. 11. r** “ i “ “ n/z-> 160165170175180185190195200205210215220225230235 240 245 250
02721.D HP022102.M Fri Mar 01 10:07:54 2002 Page 15
NYC-WTC_000011025
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NYC-WTC_000010947
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010907
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010867
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010927
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010987
Gas chromatography-mass spectrometry analysis of sample AE02719 performed March 5, 2002, reporting other unknown compounds and surrogate 2,4-DDD recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010887
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010066
GCMS laboratory results for sample AE01547 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010126
GCMS laboratory results for sample AE01638 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000010837
Administrative record from DEP Box 14 covering the period of February to March 2002 regarding World Trade Center environmental activities.
Filed in the same folder
NYC-WTC_000010838
Technical log recording laboratory parameters and counts for sample AE02713 processed in late February 2002.
Filed in the same folder
NYC-WTC_000010843
Laboratory report documenting a blank run for gas chromatography-mass spectrometry analysis of sample AE02713.
Filed in the same folder
NYC-WTC_000010862
Laboratory report documenting a reference standard run for gas chromatography-mass spectrometry analysis of sample AE02713.
Filed in the same folder
NYC-WTC_000010867
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.
Filed in the same folder