GCMS blank analysis for sample AE00555, Jan-Feb 2002

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Laboratory report showing GCMS blank analysis results for sample AE00555 conducted between January 29 and February 1, 2002.

NYC-WTC_000051512–000051530

Folder label: “GCMS X 1/9/02 A 1/29/02”

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NYC 9/11 Public Portal Document

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- Data File : C:\MSDCHEM\1\5973N\02JAN29\0109B.D Vial: 1 Acq On : 29 Jan 2002 10:31 am Operator: Sample : lab blank 1/9 Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 4-Amino-5,5-dimethyl-2-meth... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.

29.68 0.04 ug/L 24567 Chrysene-dl2 30.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-Amino-5,5-dimethyl-2-methoxyca... 243 C15H17NO2 118089-29-5 5 2 7-[3,4-(Methylenedioxy)phenyl]-3... 243 C15H17NO2 000000-00-0 5 3 2-(1,3,3-trideuteroindanyl)-p-to... 243 C16H13D3S 000000-00-0 4 4 Ferrocene, [1-(hydroxyimino)ethy... 243 C12H13FeNO> 032662-56-9 4 Abundance Scan 2304 (29.678 min): 0109B.D (-) I pm/z 244.10 100.00% 244 8000

6000

4000 Tumorrt i 1 ' 1 1 i ' 1 122 207 29.40 29.60 29.80 30.00 T I'‘’I-‘•I•'* * I " 11| F111 t ' " ’ I m/z 243.10 61.38% m/z-> 60 70 80 90 100110120130140150160170180190200210220230240250 Abundance #177722: 4-Amino-5,5-dimethyl-2-methoxycarbonyl-3-phenyl-c... 244

5000 ' ‘I 11 • • i > • 29.40 29.60 29.80 30.00 m/z 122.00 28.31%

o1 11" ‘ 111" r "' r ■ ” i 167 | ' l " j > rr. ।. i > ।> 11 , 184 196 212 j. i . i । . I > । । h 11 । ■ > i i । Fi h । i > i < । b . < 11 i 11111 J m/z-> 60 70 80 90 100110120130140150160170180190200 210220230240250 Abundance #177776: 7-[3,4-(Methylenedioxy)phenyl]-3,3a,4,5,6,7-hexah .. 243 ■ ■ i ■ ‘ 1 ■ । ’ 1 ■ ■ i ■ ■ 29.40 29.60 29.80 30.00 5000 m/z 207.10 23.49% 77 122 103 131 | 145 161 200 214 I il NAi AANJ <' I > ■11 <1 >111' । ■ 11 rl I....... " i1"1 r1" i1" • i r TTI’T n/z—> 60 70 80 90 100110120130140150160170180190200 210220230240250 Abundance #174391: 2-(1,3,3-trideuteroindanyl)-p-tolylsulphide 1 FIn — I 120 29.40 29.60 29.80 30.00 m/z 121.40 21.13%I

5000 243

65 799]...... | "11" ■ ■ IH "i" " i11" । ' i"1 144 -pHTTTTpTTT * ' | 1 ' 1 ’ I ‘ 1 ' ' I * ’ ‘ 1 I r r m/z—> 60 70 80 90 100 110120130140150160170180190 200 210 220 230 240 250 29.40 29.60 29.80 30.00

0109B.D SCAN508.M Wed Jan 30 09:02:34 2002 Page 15

NYC-WTC_000051529

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NYC-WTC_000051529Source: NYC Law Department, mirrored locally

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GCMS blank results for sample AE00830, Feb 2002 · Box DEP Box 28

NYC-WTC_000052029

Laboratory report showing GCMS blank analysis of sample AE00830 with compounds below detection limits.

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