GCMS analysis results for sample AD31674, Jan 25 2002

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Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050276–000050293

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN22\31674.D Vial: 2 Acq On : 22 Jan 2002 3:30 pm Operator: * Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-Amino-5,5-dimethyl-2-meth... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 29.67 0.10 ug/L 64358 Chrysene-dl2 30.50 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Amino-5,5-dimethyl-2-methoxyca... 243 C15H17NO2 118089-29-5 5 0 2 10-( 3'-Pyridyl)-9-oxadispiro[[2... 243 C14H13NO3 000000-00-0 5 (-070 3 6-Deoxyhemigossypol $$ 1-Naphtha... 244 C15H1603 055824-28-7 5 At 4 7-[3,4-(Methylenedioxy)phenyl]-3... 243 C15H17NO2 000000-00-0 5 Abundance Scan 2303 (29.667 min): 31674.D (-) m/z 244.10 100.00% 2-4

5000 64

108 122 198 ■ ■ • ■ i • ■ ■ • । ■ ■ 11 i ' ‘ ■ ■ । ■ ■ ■ >

49 29.40 29.60 29.80 30.00 -t 1 ■ ■ । ‘1 • • । ■ 1' ■ । ■ • ■ ■ । ‘ ' । ■'' ■ । ■ ■ ■11 • ■ ■ ■ । • ■ • ■ । m/z 243.10 52.68% •n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #177722: 4-Amino-5,5-dimethyl-2-methoxycarbonyl-3-phenyl-c... 2-4

5000 ' ' 29.40 29.60 29.80 30.00 m/z 64.00 50.82%

n/z-> 0- 40 ............... . I 60 80 100 120 140 160 180 200 220 240 Abundance #177649:10-( 3'-Pyridyl)-9-oxadispiro[[2.1.2.3]decane-4,8... 2-3

29.40 29.60 29.80 30.00 5000 130 m/z 122.10 21.55% 198 215 68 78 105 175 ' ‘ i ‘ ■ i ■ ■ ■ ■ i ■ ■ ' ■ i ■ ■ ■ ■ i ■ ‘ ' I 1 ' 1 1 I ' ' 1 " I 1 ' ' 1 I '' ■ ■ i ‘ ‘ i ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #179164:6-Deoxyhemigossypol $$ 1-Naphthalenecarboxaldehyd... - • i • • • ■ i ‘ < ' i ' 1 1 1 i 1 1 2-4 29.40 29.60 29.80 30.00 m/z 198.00 17.13% 226 5000

183 198 211

mz—> * • I ' ‘ 40 ‘ I * 60 111’1* 80 100 120 17139 15,.. 140 160 * I ‘ ’ 4 ‘ l ‘ TT i 11 ■ ■ i 180 200 220 240 ’ I***I’ * * l ‘ ‘ * I ’ ‘ 29,40 29.60 29.80 30.00

31674.D SCAN508.M Thu Jan 24 14:00:13 2002 Page 13

NYC-WTC_000050292

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NYC-WTC_000050317

Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

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