NYC 9/11 Public Portal Document
Library Search Compound Report
’ Data File : C:\MSDCHEM\1\5973N\02FEB27\02383.D Vial: 4
Acq On : 27 Feb 2002 1:13 pm Operator:
Sample : 508 scan Inst : Instrumen
Mise 2002
: February 2 7, Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator)
Title : 508 scan method
Library : C:\DATABASE\WILEY7N.L
*********************************************************************
Peak Number 8 6-amino-2-(methylamino)-4(3... Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
16.55 0.03 ug/L 21089 Acenaphthene -dl0 18.34
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 6-amino-2-(methylamino) -4(3H)-py... 140 C5H8N40 089181-81-7 5
2 Methylphloroglucinol 140 C7H803 000000-00-0 5
3 2-DIMETHYLAMINO-4,5-DIMETHYLOXAZ... 140 C7H12N20 073777-29-4 5
4 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 5
Abundance Scan 1167 (16.548 min): 02383.D (-) m/z 140.10 100.00%
140
5000
56 71
43 172
86 122 ■ ' I 1 1 ■ 1 i ■ 1 ' ' 1 1 1 1 1 I ' 1 1 1 1 1
— 16.20 16.40 16.60 16.80
0- 11 11 ■ ■ i 1 ■ 1 ■ i 1 ‘11‘111T111111‘I1 ■111' i *'' ■ ।' r m/z 71.10 37.34%
m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170
Abundance #35082: 6-amino-2-(methylamino)-4(3H)-pyrimidinone
140
5000 57 111
43 16.20 16.40 16.60 16.80
95 m/ Z 56.10 35.82%
85
67
0- ' • i 1 ■ ■ i ■ ■ ■ ■ । > i ■ > > ■ i ■ ■ ■ ■ i ■ ■ ■ < । ■ • ■ ■ । 1 ■ i ■ ■ ■ ■ i11 i1 1 ■' i' ■ ■1 i n
m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170
Abundance #35391: Methylphloroglucinol
no
-
16.20 16.40 16.60 16.80
5000 m/ z 136.00 32.50%
111 123
66 85 94
0- -n-p-r 11 " I''1111'1111 ri' 11
m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170
Abundance #35418: 2-DIMETHYLAMINO-4,5-DIMETHYLOXAZOLE $$ 2-Oxazolami... 1 1 i ‘ ' 1 i ' ' i ' ' 1 1 i ■ ' ' ' i '
140 16.20 16.40 16.60 16.80
m/z 138.00 30.30%
44
5000 56
72 125
97 111
0- TIII ’ I 1 ' 1 ‘ I TITp 1 ' f ■ ' 1 1 I ‘ ' 1 1 ' ' 1 I ‘
m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80
32383.D HP022102.M Thu Feb 28 08:46:56 2002 Page 10
NYC-WTC_000004999
OCR can misread numbers and units. Confirm readings against the page image before using them.