DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report - Data File : C:\MSDCHEM\1\5973N\02FEB26\0130B.D Vial: 1 Acq On : 26 Feb 2002 10:17 am Operator: Sample : lab blank 1/30 Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Methylphloroglucinol Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 16.55 0.02 ug/L 19273 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methylphloroglucinol 140 C7H803 000000-00-0 9 2 2-DIMETHYLAMINO-4,5-DIMETHYLOXAZ... 140 C7H12N20 073777-29-4 9 3 1,3,5,7-Tetraazatricyclo [3.3.1.1. .. 140 C6H12N4 000100-97-0 7 4 2,5-DIMETHYLCYCLOHEXANE- 1,4-DION... 140 C8H12O2 000583-81-3 5 Abundance Scan 1167 (16.548 min): 0130B.D (-) m/z 140.10 100.00% 140

5000 56 122 172 43 ,............ 71 84 ...... .1. 0- ‘ 1 I 11 ' ' I ' ' ■' 11 ' > । I__ I । -11' ■ ■ । ■ ’11’11’1’171111111 ■ ■ i 11 1 ' r ■1 111 11 1 i -i-r-p 16.20 16.40 16.60 16.80 m/z 138.10 35.97% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35391: Methylphloroglucinol 14.0

5000 ' 1 i ' ' ■ - । । 1 । ' । ■ I । 111 123 16.20 16.40 16.60 16.80 85 94 m/ Z 172.20 31.43% 66 0- ■ ।'1111' ■' ।1 TT-p ■ ■ i'' 1' ' ' i' ’ 1 ' i 1 '' ' i 1 ' ' ' i' m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35418: 2-DIMETHYLAM1NO-4.5-DIMETHYLOXAZOLE $$ 2-Oxazolami... 140 16.20 16.40 16.60 16.80 5000 44 m/z 122.10 29.71% 56 125 72 97 111

O-TTTTT ■ ■ i ■ ■ ■ 11 ■ ■ ■ 11 ’ 7:1’41 ■ -111 ■ ■ ■ • II > 111A1111 11t111111111711117711 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35199:1,3,5,7-Tetraazatricyclo[3.3.1.1(3,7)]decane (CAS)... 42 16.20 16.40 16.60 16.80 m/z 56.10 27.45% 5000 140

49 84 — 112 35 — 98 I 01'i' ‘ i '11 ■ ■j 11 ■ ■1 ■ ।11'11' ■ ■11 ■ ■ ■ Fi’l’i ‘ 11111111 i11 •' r ■111111 ■ [ m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

0130B.D HP022102.M Wed Feb 27 08:34:18 2002 Page 11

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