DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound. Report Data File C:\MSDCHEM\l\5973N\02FEB26\0130B.D Vial: 1 Acq On 26 Feb 2002 10:17 am Operator: Sample lab blank 1/30 Inst : Instrumen Mise February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 1,3-Benzenedicarboxylic aci... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 18.73 0.04 ug/L 27663 Acenaphthene-dl 0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Benzenedicarboxylic acid, 5-... 180 C9H804 000499-49-0 5 2 7-Methyl-2 ,3,6,7-tetrahydrocyclo... 163 C10H13NO 000000-00-0 5 3 2-Formylthieno[3,2-b]pyridine $$... 163 C8H5NOS 094191-18-1 5 4 1,4-Benzenedicarboxylic acid, 2- . 180 C9H804 005156-01-4 5 Abundance Scan 1360 (18.727 min): 0130B.D (-) m/z 162.10 100.00% 162

49 180 80 5000

18.40 18.60 18.80 19.00 OT 111 ■ ‘111'1 ■ ।1 i1 11' i ■ ' 1 1 11 ■1 ■ i ■ ■' ■ i' 1 ' ■ i m/z 180.10 67.50% /z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #85810:1,3-Benzenedicarboxylic acid, 5-methyl- $$ Isophth... 180 163

5000- 135 i ‘ ■ i 77 18.40 18.60 18.80 19.00 89 m/z 49.00) | 63.28% 105 119 151 । \ 0 - ______ I______ — ’1’11’1/1 ....... T’i N /z- > 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #63397: 7-Methyl-2,3,6,7-tetrahydrocyclopent(b)azepine-8(1... 162 + "II ■ ■ i ' ' 18.40 18.60 18.80 19.00 5000 m/z 163.10 56.86%

65 77 91 106 120 148

/z-> 0- 40 ......... Il... |l *.. ।.. „ ■11 ■ ■ ‘1 ।11 ' 111 50 60 70 80 90 100 110 120 130 140 150 160 170 180 134 i ■ ■' 11

- Abundance #63123: 2-Formylthieno[3,2-b]pyridine $$ Thieno[3,2-b]pyri... 162 18,40 18.60 18.80 19.00 m/z80.10 50.91%

5000 134 63 82 90

m/z-> 0 ।1 ■111 ■ ■ ■' । ■ ■ ■ ■ ।'11 40 50 60 70 80 90 ‘' i ■ ■ ■ ■ i'1' ■ i ■ ■'111 L 100 110 120 130 140 150 160 170 180 ■ ■ i1 ■ ‘ ■ i ■ ■ ■ ■ i 18.40 18.60 18.80 19.00

0130B.D HP022102.M Wed Feb 27 08:34:18 2002 Page 12

NYC-WTC_000004521

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NYC-WTC_000004521Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999