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GCMS analysis results for sample AE00838, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.

NYC-WTC_000052167–000052186

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052183
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00838.D Vial: 2 Acq On : 31 Jan 2002 3:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 1,2-Benzenedicarboxylic aci... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

19.99 0.10 ug/L 82668 Acenaphthene-dl0 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual 000131-70-4 53 P, 1 1,2-Benzenedicarboxylic acid, mo... 222 C12H1404 2 1,2-Benzenedicarboxylic acid, mo... 222 C12H1404 000131-70-4 50 C 3 1,2-Benzenedicarboxylic acid, mo... 222 C12H1404 000131-70-4 50 4 Benzene, l-isothiocyanato-2-meth... 149 C8H7NS 000614-69-7 47 Abundance Scan 1455 (19.985 min): 00838.D (-) m/z 149.00 100.00% 149 fl 5000 71 177 TIT ′′′′′′ 43 « _ 93 I" 19.60 19.80 20.00 20.20 20.40 0- 11.../.55..1L 84 1 11'1' I' * ‘' I " 122 r ■ " i' ■ " i "" i"" ..... ... m/z 71.10 31.22% m/z—> 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 Abundance #147073:1,2-Benzenedicarboxylic acid, monobutyl ester (CA... 149

5000 56 ' I • ’ ’ I A. 19.60 19.80 20.00 20.20 20.40 m/z 177.10 24.78% 41 65 76 93 105 122 ■n/z-> 0- 'I""!1 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 I 167 i” • • i • •" r " ■ i 222

Abundance #147069:1,2-Benzenedicarboxylic acid, monobutyl ester 149

19.60 19.80 20.00 20.20 20.40 5000 m/z 176.00 15.41%

— 56 65 76 93 1 05 122 167 0 I 222 ' ■" i ■H ■ r'" r "11" " i'" ■ i ■'" i" " i' n/z-> 30 40 50 60 70 80 90 100110120130140150160170180190200 210220230 Abundance #147072:1,2-Benzenedicarboxylic acid, monobutyl ester TT I ' ' ' ' I ’ ' 149 19,60 19.80 20.00 20.20 20.40 m/z 43.10 12.02%

5000 56

m/z-> 0 65 76 93 105 mprelp n... I1...... Ii 167 | 122 222 TpTTTpTT-rTTTTTpT-rrpTTTYI-I-nT^ 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 MAMMMbMdnushauut 19.60 19.80 20.00 20.20 20.40

00838.D SCAN508.M Fri Feb 01 09:19:07 2002 Page 13

NYC-WTC_000052183

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NYC-WTC_000052183Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗

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