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GCMS analysis results for sample AE00838, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.

NYC-WTC_000052167–000052186

Folder label: “GCMS X 1/11/02 A 1/31/02”

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Scanned page image, NYC-WTC_000052182
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00838.D Vial: 2 Acq On : 31 Jan 2002 3:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 10 3,5-Difluoroacetonitrile Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 18.42 0.13 ug/L 102156 Ac enapht hene-d10 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3,5-Difluoroacetonitrile 153 C8H5F2N 122376-76-5 9 PC 2 Hydrazine, (4-nitrophenyl)- (CAS... 3 Eicosane 153 282 C6H7N3O2 C20H42 000100-16-3 9 000112-95-8 9 CUov v 4 Ethanone, 1-[3-[[5-(3,3-dimethyl... 288 C18H24O3 106929-49-1 9 Abundance Scan 1318 (18.421 min): 00838.D (-) m/z 154.10 100.00% 57 154

43 71 5000 85 — 99

n/z-> 01 40 4 60 80 100 120 140 160 180 200 220 240 260 280 18.00 18.20 18.40 18.60 18.80 m/z 153.10 95.28% Abundance #50840: 3,5-Difluoroacetonitrile 1$3 126

5000 T-TBU I I I I I I 18.00 18.20 18.40 18.60 18.80 31 63 75 m/z 57.10 92.41% 107 । । o1 .1........ 1 ‘ I’ ’’ I ' I............. ....... n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #50642: Hydrazine, (4-nitrophenyl)- (CAS) $$ P-NITROPHENYL... 1$3 AAAA 18.00 18.20 18.40 18.60 18.80 5000 m/z 43.05 55.45% 50 65 77 90 123 138

n/z-> 0 _L 40 60 107 ........................................................ ................... 80 100 120 140 160 180 200 220 240 260 280 Abundance #228988: Eicosane I ' ' 1 ' I ' ' ' * 1 1 ’ ' ' I........ .. I* ' 1 57 18.00 18.20 18.40 18.60 18.80 43 m/z71.10 52.08% 71 5000 85

99

m/z-> 0 T-r-p-r 40 LAX 10011 113120127 140141 155160169180 200 220 240 260 280282 60 80 18.00 18.20 1840 18.60 18.80

00838.D SCAN508.M Fri Feb 01 09:19:07 2002 Page 12

NYC-WTC_000052182

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NYC-WTC_000052182Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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machine-extracted · confidence unavailable · Check page ↗

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