GCMS surrogate recovery results for sample AE03184, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02MAR01\03184.D Vial: 4 Acq On : 1 Mar 2002 12:48 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************** Peak Number 6 2,3,4,5-Tetrahydropyridazine Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 4.86 0.23 ug/L 81939 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,3,4,5-Tetrahydropyridazine 84 C4H8N2 000694-06-4 2 2 Cyclopentanone 84 C5H80 000120-92-3 32 3 3,4-Dihydropyran $$ 2H-Pyran, 3,... 84 C5H80 000110-87-2 9 4 Cyclopentanone (CAS) $$ Dumasin ... 84 C5H80 000120-92-3 9 Abundance Scan 132 (4.864 min): 03184.D (-) m/z 83.95 100.00% 84

55 5000- 41 59

4.60 4.80 5.00 5.20 | 01 '' i1'' ' i ■ ‘ ■ ■ i'''' i 1 ■' ■ i 111’11-1111111171111111 ।1 ■ ■11 ■ m/z 55.10 57.12% mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3177:2,3,4,5-Tetrahydropyridazine 84

29 .. 5000 55 41 4.601 4.80 5.00 5.20 26 69 m/ z 41.10 45.12% 44 0! '11' ‘ ‘ i ■' i ‘'11 ’ 144’11’4 11 ■' ■11 ■ ■1 * ।' ■ i'1 ■ ■ i'1 mfz~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3268: Cyclopentanone 55 4.60 4.80 5.00 5.20 5000 41 84 m/z 59.10 41.61% 27

1 38

m/z-> Of m' 20 25 TTfT 50 -HH 110— 30 35 40 45 50 55 60 65 70 75 80 I'"'I" 85 90 Abundance #3373:3,4-Dihydropyran $$ 2H-Pyran, 3,4-dihydro- (CAS) ,.......... 55 4.60 4.80 5.00 5.20 m/z 83.00 39.82% 27 5000 84

42 45 51 । . 69 0 '' i ■'' ■ i ■ ■ i' ■1 ■ i11111111111 n|l ■ -T TmT /z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20

)3184.D HP022102.M Mon Mar 04 12:32:53 2002 Page 8

NYC-WTC_000006056