GCMS results for sample AE00469, Jan 24 2002

NYC 9/11 Public Portal Document

Library Search Compound Report:

Data File : C:\MSDCHEM\1\5973N\02JAN11\00469.D Vial: 8 Acq On : 11 Jan 2002 7:55 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 2,3,4,5-Tetrahydropyridazine Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 4.85 0.15 ug/L 59324 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,3,4,5-Tetrahydropyridazine 84 C4H8N2 000694-06-4 45 2 2H-Pyran, 3,4-dihydro- $$ .delta... 84 C5H80 000110-87-2 9 3 Cyclopentanone 84 C5H80 000120-92-3 9 4 (E)-1-Propenylaziridine $$ Aziri... 83 C5H9N 080839-91-4 9 Abundance Scan 129 (4.847 min): 00469.D (-) m/ z 83.95 100.00% 84

55 5000 41 59

-+ 51 4.40 4.60 4.80 5.00 5.20 0 '' i ■ ■ ■ ' i'1 1 TTrV1111 I " 111 " " I' ■ । ■ ■ • ■ । ■1 । ■ ■ ■11 ■ m/z 55.10 54.20% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3177: 2,3,4,5-Tetrahydropyridazine 84

29 5000 55 41 4.40 4.60 4.80 5.00 5.20 26 69 m/z 41.10 40.16% 44 ।

/z-> 0 '11 ■' ■ ■ i 20 25 30 35 40 H45...... Ill • • i ■ > > ■ i ■ ■ 50 55 60 65 70 75 80 85 90 i ■ ■ ■ • । ■ i ■ ■ i ■ ‘ ■ i1 1

Abundance #3369: 2H-Pyran, 3,4-dihydro- $$ .delta.(Sup2)-Dihydropyra... 55 44 A 4.40 4.60 4.80 5.00 5.20 27 84 m/ z 83.10 38.59% 5000

69

m/z- > 0 1 ■ r 1 ■ ■ i —451 I - ........... ... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3268: Cyclopentanone 55 4.40 4.60 4.80 5.00 5.20 m/z 59.10 38.03% 5000 41 84 27

38 50 0 111 ■1 ■' i1 11 I " 11111111 ' -- 1 ■ ■ i ■1' ' I' '1 ■ 11 ■ ' ■ i' '1 ' i r ' TT ‘ 1 1 1 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.40 4.60 4.80 5.00 5.20

00469 .D SCAN508.M Mon Jan 14 10:47:11 2002 Page 4

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