GCMS results for sample AE00469, Jan 24 2002

NYC 9/11 Public Portal Document

Llbrary Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00469.D Vial: 8 Acq On : 11 Jan 2002 7 : 55 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 3 Butenol, methyl- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.10 ug/L 40068 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butenol, methyl- 86 C5H10O 060766-00-9 72 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 50 3 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 45 4 Trifluoroacetic acid, 2-tetrahyd... 198 C7H9F3O3 000000-00-0 33 Abundance Scan 143 (5.006 min): 00469.D (-) m/ z 71.10 100.00% 43 71

5000 55 59 39 —--A------- m/z-> 0b 5 TT LL. 51 i ■ ■ ■ ■ i ■ • 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 84 —mmmPPPPP 4 60 m/z 4.80 43.10 5.00 5.20 5.40 93.12% Abundance #4093: Butenol, methyl- 43 7

5000 59 27 4.60 4.80 5.00 5.20 5.40 15 31 m/ Z 41.10 60.29% 53 TTI "' i'1" i1' mHH IPH —P T TTTTTMIN) 671 86 0b TI’T miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4083: 3-Buten-2-ol, 2-methyl- 71 — 43 4.60 4.80 5.00 5.20 5.40 5000 m/z 69.10 48.30% 59 27 31 53

m/z-> ob -7 -HH mH +..86.... r 11" " i " 1' I' " ' i' TIT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4081: 3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... 7h 4.60 4.80 5.00 5.20 5.40 m/ z 59.00 45.51% 43 5000 59 27 31 67 53

/z-> 0bTT’UUIUnr '' I'111111" 111 5 1 — ,। "I" "I1‘"I86 1'"I 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ------ 4.60 4.80 5.00 5.20 5.40

00469.D SCAN508.M Mon Jan 14 10:47:11 2002 Page 5

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