Gas chromatography-mass spectrometry analysis of sample AE00327 showing unknown compounds and surrogate 2,4-DDD measurement.
NYC-WTC_000051192–000051205Folder label: “GCMS X 1/8/02 A 1/10/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Llbrary Search Compound Report
Data File : C:\MSDCHEM\1\5973N\02JAN10\00472.D Vial: 7 Acq On 10 Jan 2002 7:46 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2-Buten-l-ol , 3-methyl- (CA... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.
4.63 0.16 ug/L 54275 1,4-Dichlorobenzene-d4 9.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Buten-I-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 2 2-Buten-I-ol, 3-methyl- $$ .gamm... 86 C5H10O 000556-82-1 3 2-Buten-1-ol, 3-methyl- 86 C5H10O 000556-82-1 47 4 2-Buten-1-ol, 2-methyl- (CAS) $$... 86 C5H10O 004675-87-0 40 Abundance Scan 110 (4.630 min): 00472.D (-) m/z 71.10 100.00% 41 71 88 57
5000 53 68 85 14 4.20 4.40 4.60 4.80 5.00 49 m/z-> 0 f >T> ' | I ' M f, 4 ! | p , 20 25 gaannluve 30 35 40 45 50 55 60 65 70 75 80 85 90 ■ i • TTT 111 FFUTTT 95 m/ z 41.10 93.97%
Abundance #4075: 2-Buten-1-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 7h 41 5000; 53 86 AAA. 4.20 4.40 4.60 4.80 5.00 67 m/z 88.00 88.43% 83, /z-> ol '' i'' ■ ■ ir' '' i'' '' i' T’I 20 25 ........ ............... TT-p 30 35 40 45 50 55 60 65 70 75 80 85 + 111 ‘d 11 ■ • 90 95 Abundance #4067: 2-Buten-1-ol, 3-methyl- $$ gamma., gamma.-Dimethyl... 71 4.20 4.40 4.60 4.80 5.00 5000 m/z 57.10 72.42% 53 27 86 31 67
n/z-> 01 -n-p-m-p- 20 25 30 35 59 ITTTTT+ 40 45 50 55 60 65 70 75 80 85 + . .............. T-p-T-r-r-p-r
90 95 Abundance #4074: 2-Buten-1 -ol, 3-methyl- 71 4.20 4 40 4.60 4.80 5.00 m/z 43.10 43.59%
5000 39 53 67
27 86 42 50 — m/z-> 0 ‘' i' " ' i' '111' 1111 ।1 i •1" ।1 20 25 30 35 40 45 50 ' i111 ■ i' " ' r 55 60 65 + 70 —mm ■ 75 80 85 90 95 4.20 4.40 4.60 4.80 5.00
0472.D SCAN508.M Fri Jan 11 10:08:55 2002 Page 5
NYC-WTC_000051198
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000051088
Laboratory report showing GCMS analysis of sample AE00309 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051055
Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051422
Laboratory report showing GCMS analysis of sample AE00463 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051105
Laboratory report showing GCMS analysis of sample AE00318 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051301
Laboratory report showing GCMS analysis of sample AE00471 with surrogate recovery data on January 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051408
Laboratory report showing GCMS analysis of sample AE00462 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050793
Laboratory report listing unknown compounds and surrogate recovery for sample AE00105 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049929
Laboratory report showing GCMS analysis of sample AD31637 including unknown compounds and surrogate recovery data.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051439
Laboratory report showing GCMS analysis of sample AE00464 with surrogate recovery data on January 24, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051073
Laboratory report showing GCMS analysis of sample AE00308 for unknown compounds and DDD on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049990
Laboratory report showing GCMS analysis of sample AD31644 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006045
Analytical report showing surrogate recovery data for sample AE03184 analyzed on March 15, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051152
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051153
Document header page containing identification codes and metadata for GCMS files processed in early January 2002.
Filed in the same folder
NYC-WTC_000051156
Laboratory report detailing GCMS analysis of sample AE00327 for volatile organic compounds on January 10-11, 2002.
Filed in the same folder
NYC-WTC_000051165
Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.
Filed in the same folder
NYC-WTC_000051179
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 10-11, 2002 testing.
Filed in the same folder