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GCMS analysis results for sample AE00562, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00562 conducted on February 1, 2002.

NYC-WTC_000051567–000051585

Folder label: “GCMS X 1/9/02 A 1/29/02

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Scanned page image, NYC-WTC_000051575
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN29\00562.D Vial: 4 Acq On : 29 Jan 2002 1:02 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2-Buten-l-ol, 3-methyl- (CA... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

4.63 0.15 ug/L 69459 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm ■ CAS# Qual

1 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 43 2 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 43 3 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 16 4 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 12 Abundance Scan 110 (4.630 min): 00562.0 (-) m/z 71.10 100.00% 41 57 71 88

5000

47 101 N............ 1. 4.20 4.40 4.60 4.80 5.00 + TT t1' *' l " *' i l ′ ‘ ‘I m/z 57.10 86.13% n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4075: 2-Buten-1 -ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 71 41

5000 .1 ■ 53 4.20 4.40 4.60 4.80 5.00 86 m/ z 88.00 85.07% TOTUCIPUTCUTTT । ' I ’ ’11111 70201002111277/7 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4076: 2-Buten-1-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL...

41 71 MM... fl 4.20 4.40 4.60 1 ' | ' ri ’"I"' 1 ' 4.80 5.00 5000 m/z 41.10 83.66% 53 86 27

" i " ‘11 ‘ ,lr'T'" 'i""i • । ■ ■ ■ • । ■ ■ • ■ । ■ 1111 —TTTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4070: 2-Buten-1 -ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 43 53 27 86 5000 67

m/z--> " i " " i' TIT TTT I' " 59 । ■ ■ ■ ■ । 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 I’ THT 72 TT _AAnA 4.20 4.40 4.60 4.80 5.00

)0562 .D SCAN508.M Wed Jan 30 09:02:02 2002 Page 5

NYC-WTC_000051575

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NYC-WTC_000051575Source: NYC Law Department, mirrored locally

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