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GCMS analysis results for sample AE03246, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03246 conducted on March 15, 2002.

NYC-WTC_000006105–000006125

Folder label: “GCMS X 2/12/02 A 3/01/02

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NYC 9/11 Public Portal Document Library Search Compound Report . Data File C:\MSDCHEM\1\5973N\02MAR01\03246.D Vial: 1 Acq On 1 Mar 2002 4:00 pm Operator: Sample 508 scan Inst : Instrumen Mise March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 2-Buten-l-ol, 3-methyl- (CA... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 4.64 0.18 ug/L 86539 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 49 2 2-Buten-I-ol, 2-methyl- (CAS) $$... 86 C5H10O 004675-87-0 47 3 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 38 4 2-Buten-l-ol, 3-methyl- $$ .gamm... 86 C5H10O 000556-82-1 38 Abundance Scan 112 (4.638 min): 03246.D (-) m/z 71.10 100.00%

o 41 71 57 88

5000

101 . ..... M. 4.20 4.40 4.60 4.80 5.00 84 m/z 41.10 98.01% 0 ■ ■ । ■1 - ■ ।1 ■ ■ 11 ■ ■ ■11 ■ ■ ■ ■ । ■ । ■ •' ■ । ■1111 " i " 111 mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4075:2-Buten-1-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 7|1 41

5000 53 4 4.40 4.60 4.80 5.00 4.20 86 m/z 88.00 68.85%

miz-> 0 " i " " i1" ' i " " i1 ‘ " i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 + i " ‘' i

Abundance #4064: 2-Buten-1-olt 2-methyl- (CAS) $$ 2-Methyl-but-2-ene... 71 1’’’ 4.20 4.40 4.60 4.80 5.00 5000 43 86 m/ z: 57.00 67.52% 11 53

niz-> Of ' ‘ i " " I' " ‘ ir ■ " i " ■ IPT PArll. — 1" I " " I ‘1111" " 11T111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4076: 2-Buten-1-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 71 4.20 4.40 4.60 4.80 5.00 m/z 43.10 55.31% 41 5000 53 86 27

m/z-> 0 Ti i"111' " i " ‘11" ■ i11" i" —mm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 '" i" " i" " i '" I" " I" " I" " I" " I AAMA 4 20 4.40 4.60 4.80 5.00

>3246.D HP022102.M Mon Mar 04 12:33:13 2002 Page 7

NYC-WTC_000006115

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NYC-WTC_000006115Source: NYC Law Department, mirrored locally

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