GCMS analysis results for sample AE03246, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02MAR01\03246.D Vial: 1 Acq On : 1 Mar 2002 4:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Carbonic acid, dihexyl este... Concentration Rank 7 R.T. EstConc Area Relative to I STD R.T. 4.25 0.17 ug/L 82547 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Carbonic acid, dihexyl ester $$ ... 230 C13H2603 007523-15-1 42 2 Pentane, 2-bromo-4-methyl- 164 C6H13Br 030310-22-6 39 3 Methacrylamide 85 C4H7NO 000079-39-0 38 4 Methacrylamide $$ 2-Propenamide, ... 85 C4H7NO 000079-39-0 38 Abundance Scan 78 (4.254 min): 03246. D (-) m/z 85.0.0 100.00% 41 85

5000 60 l\...... A., 4.00 4.20 4.40 4.60

mz-> 0- 1′111411 4 1 ′ ′ 1‘‘I 10 20 30 40 .5.11 50 60 70 80 90 100 110 m/z 41.10 80.34% Abundance #159657: Carbonic acid, dihexyl ester $$ Dihexyl carbonate... 85

5000- 41 56 AAAA. 4.00 4.20 4.40 4.60 27 m/z 43.10 50.39% 69

m/z-> 0—T 10 111 T ---------------- 20 30 40 50 60 70 80 s.. 1 -3— 63 |

90 100 110 Abundance #63838: Pentane, 2-bromo-4-methyl- .... ...... 43 A M/W r 85 4.00 4.20 4.40 4.60 5000 m/ z 60.00 33.60% 27 69 15 57

mz-> O—TIT | 1 ' I ' * ‘ ' I 1 1 37 20 30 ‘‘ I 40 + *II—m——OTT Il.....................80 ■ ' i ' ■ 107 10 50 60 70 80 90 100 110 Abundance #3601: Methacrylamide - • i > ■ ■ ■ i ■ > . . । . . . . । . 41 85 4.00 4.20 4.40 4.60 m/ z; 42.10 18.91% 1 5000 69 ........ . m/z-> 0 1 । । 1 1 1 1 I ' 1 1 ’I 1 1 11r' 10 20 30 40 46.,50... 60 70 80 90 100 110 4.00 4.20 4.40 4.60

)3246.D HP022102.M Mon Mar 04 12:33:13 2002 Page 6

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