GCMS results for sample AE00699, Jan 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN16\00699.D Vial: 4 Acq On : 16 Jan 2002 1:20 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 2 2-Propenoic acid, 2-methyl-... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

4.24 0.11 ug/L 34564 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm • CAS# Qual

1 2-Propenoic acid, 2-methyl- (CAS... 86 C4H602 000079-41-4 30 2 4,7,10,13,16-Pentaoxanonadeca-1,... 274 C14H2605 058185-54-9 28 3 Cyclopropanecarboxylic acid (CAS... 86 C4H602 001759-53-1 25 4 N-Hydroxymethylacetamide $$ Acet... 89 C3H7NO2 000625-51-4 10 Abundance Scan 76 (4.241 min : 00699.D (-) m/z 85.00 100.00% 86 41

5000 60 49 3.80 4.00 4.20 4.40 4.60 o1 ■ i 11 1 1 i 1 ‘ "IIt ■ 1 i ■ ■ m/z 41.10 75.69% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #3758:2-Propenoic acid, 2-methyl- (CAS) $$ Methacrylic ac... 41 85

5000 aA4 3.80 4.00 4.20 4.40 4.60 69 m/z 43.10 72.81% । .- 58 0• । ' . ' . । ■ ------------------ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #218196: 4,7,10,13,16-Pentaoxanonadeca-1,18-diene 4 3.80 4 00 4.20 4.40 4.60 5000 m/z 87.10 35.07% 73 85 59 133 103 117 O' | 1 1 1 1 | । —HHr 11,11 n i ! |U. —— m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #3763: Cyclopropanecarboxylic acid (CAS) $$ Carboxycyclopr... 11 I ........ I1 r TTr TIT 4 3.80 4.00 4.20 4.40 4.60 85 m/z 39.10 31.84%

5000 58 69 27

m/z-> O—TT TI " 20 I 30 40 m 50 60 — ' 90 70 80 100' 110 120 130 140 3.80 mmO’T—TETT’T 4.00 4.20 4.40 4.60

00699.D SCAN508.M Thu Jan 17 08:17:00 2002 Page 4

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