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GCMS results for sample AE00699, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00699 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000052001–000052016

Folder label: “GCMS X 1/10/02 A 1/16/02

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Scanned page image, NYC-WTC_000052009
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN16\00699.D Vial: 4 Acq On : 16 Jan 2002 1:20 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2-Buten-l-ol, 3-methyl- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

4.63 0.10 ug/L 32158 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm . CAS# Qual

1 2-Buten-l-ol, 3-methyl- 86 C5H10O 000556-82-1 53 2 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 50 3 2-Buten-l-ol, 3-methyl- 86 C5H10O 000556-82-1 45 4 3-Penten-2-ol $$ .alpha.,.gamma.... 86 C5H10O 001569-50-2 42 Abundance Scan 110 (4.630 min): 00699.D (-) m/z 41.10 100.00% 4h 71 57 88

5000 53 44 49 67 85 1 . 4.20 4.40 . . . 4.60 4.80 5.00

n/z-> 0) 20 11 ‘111111 ' i1 ■' ■ i1 ■ ■ 25 30 35 40 XX 45 50 55 60 65 70 TTI’ 75 80 85 "Tttrrir 90 95 m/z 71.00 90.18% Abundance #4074: 2-Buten-1-ol, 3-methyl- 7h

5000 39 53 67 1 f1 '■1 ■ । ■ ■ ■ 1 । — 4.20 4.40 4.60 4.80 5.00 86 m/ z 57.20 66.47% 27 42 50 a 01 ‘‘‘‘11 nz->_ ‘ 20 TTTTTTT + - 'I' IT* 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ' i11 ’11 ■'1111 IT Abundance #4071:2-Buten-l-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 7h 1′110/000/1/1 39 53 4.20 4.40 4.60 4.80 5.00 67 5000 27 m/z 88.10 64.90% 86 31 42 49 59 Of 1 ■ r ■ ■' i ■ ■ ■ । L ■ ■ i • l ■ TIITTTTT TTT r mA —mPPPTPTTT D1T rn/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4068:2-Buten-1-ol, 3-methyl- 7h 4.20 4.40 4.60 4.80 5.00 m/z 39.10 47.00%

5000 53 27 68 86 31 0 •*।। > ■ 11 ■ • > r111 i1 • > ■ i'11 ri *T ' rr 'I..........."I1 1^1^' l r TH—TTTTT I '''' 1 ' • ' ' "" 1 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.20 4.40 4.60 4.80 5.00

00699.D SCAN508.M Thu Jan 17 08:17:00 2002 Page 5

NYC-WTC_000052009

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NYC-WTC_000052009Source: NYC Law Department, mirrored locally

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