GCMS analysis results for sample AE00319, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN08\319.D Vial : 4 Acq On : 8 Jan 2002 7:56 pm Operator: Sample : 508scan Inst : Instrumen Mise 2002 : January 8, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 2-Buten-l-ol, 3-methyl- (CA... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

4.63 0.14 ug/L 49717 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Buten-l-ol, 3-methyl- (CAS). $$... 86 C5H10O 000556-82-1(50 2 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 47 3 2-Buten-l-ol, 3-methyl- $$ .gamm... 86 C5H10O 000556-82-1 40 4 3-PENTEN-2-OL, (Z) -_____________________ 86 C5H10O 024652-50-4 38 Abundance Scan 110 (4.630 min): 319.D (-) m/z 41.10 100.00% 41 57 71 88

5000

101 AA ... .0. A - - / 49 4.20 4.40 4.60 4.80 5.00 - i "i■ 84 m/Z 88.00 98.24% 0 " r ■ " r 1'' i1'1 ■ i i ‘111 ■ l • • 111 > > ■ ■ l ■ ■ i" ■ ■ i n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4075: 2-Buten-1 -ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 71 41 5000 53 4.20 4.40 4.60 4.80 5.00 86 m/z 71.00 92.16% o ■' r " ■ r ■ ■ ■ r ■" i ■'" i Hr... H-l' ■■।•>■■।• —p 1111"11 r1" i" ■' i" " i " " i " " i n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4076: 2-Buten-1 -ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 71 ..... AN 11.. A 41 4.20 4.40 4.60 4.80 5.00 5000 m/z 57.10 88.84% 53 86 27

Ol 11'''11'1'' I' 11 ।.. ... 1" i " '' i ■' ■' r " ■ i' ■ •' i

1.... 11 i" " i I'''' t 'i""r■ /z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4067: 2-Buten-1-ol, 3-methyl- $$ .gamma.,.gamma.-Dimethyl... 71 4.20 4.40 4.60 4.80 5.00 m/z 43.10 58.02%

5000 53 27 86

/z-> 59 66 + 0 ' 1 | I I H । I TTT ■ ■ । > ।। ■ 11 • IWTTTT ............ I 11’ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 i' ■" i " ■ ■ r " ■ i 4.20 , A AN . My ■ A M ■ A 4.40 4.60 4.80 5.00

319.D SCAN508.M Wed Jan 09 15:17:57 2002 Page 4

NYC-WTC_000051129