GCMS analysis results for sample AE00319, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN08\319.D Vial: 4 ' Acq On : 8 Jan 2002 7:56 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.49 0.23 ug/L 80094 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0/90/ 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 64 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 38 Abundance Scan 10 (3.488 min): 319. D (-) m/z 74.00 100.00% 74 82 5000 47 । ■ ■1 ■ । ■11 ■ । ■1 ■ > । 38 3.50 3.60 3.70 3.80 3.90

m/z--> Of 1 i ■ ■ ■ ■ I ■ ■ ' ■ i ■ 10 20 30 4 40 50 ______ L 60 70 ■ i ' ■

80 ■ '

90 i '

100 I........................ 110 m/z 82.00 57.17%

Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74

5000 82 i • ■ ■ ■ i > • • • i • ■ • • i 3.50 3.60 3.70 3.80 3.90 47 m/z 84.00 36.06% 35

n/z-> 0

Abundance

5000 11’ ‘I’ 10 20 1.....III,.., 30 40 50 60 __________ L ■ i ■ 1 ■ ■ i ■ 70 80 90 100 #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 7l4 TU1

82 [ 109 110

A;3.50 3.60 3.70 3.80 3.90 m/z 76.00 35.32% 47 35 12 Of । । । 11 ■ । —.. 1.. III,... __________ L TIit 1 ■ l ■ ■ ■ > I • I ■ i • ■ ■ • । 108 ■ 1 I • ■ m/z-> 10 20 30 40 50 60 80 70 90 100 110 Abundance #11644: Acetonitrile, dichloro- 74 3.50 3.60 3.70 3.80 3.90 35 m/z 47.00 25.55% 5000 82 47

m/z-> 0 ■ • । ■ ■ ■ • । ■ ■ ■ ■ । 1 10 20 30 40 । PPPt 50 60 70 80 1 ■ i ■ ■ ■ ■ i ' ■ ■ ■ i ' 90 100 110 i ■ ■' 1 i A ।11 ’11 3.50 3.60 3.70 3.80 3.90 A 319.D SCAN508.M Wed Jan 09 15:17:57 2002 Page 3

NYC-WTC_000051128