GCMS results for sample AE00314, Jan 24 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN14\00314.D Vial: 3 Acq On : 14 Jan 2002 12:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 1 Dichloroacetonitrile $$ Ace... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 3.49 0.13 ug/L 45959 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 74 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 64 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 4 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 38 Abundance Scan 10 (3.488 min): 00314.D (-) m/z 74.00 100.00% 74

82 5000 47 38 3.50 3.60 3.70 3.80 3.90 Of 1III111IIIII m/ Z 81.90 55.53% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74

82 5000 47 M• • • I i. ■ ■. i ’'' i 3.50 3.60 3 70 3.80 3.90 38 m/z 76.00 31.30% ........ I ।I ■ i ' 95 102 108 ■' ■ ■ i 1 ■ 1 1' i ' ' 0 ■ i ■ • ■ ' l ' ■ 1 ■ i ■ i ■ ' i ' ' ' ' i ■ ' ' ■ i ' m/z--> 10 20 30 4060 70 50 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 82 TTT i . ■' ’ i ■ ■ ■ ' i ' ' ' ■ i

3.50 3.60 3.70 3.80 3.90 5000 m/z 83.90 29.04% 47

v/z~> 12 0 ' 1 1 I 1 1 1 1 I 1 1 1 1 I 1 Abundance 10 20 30 -+ 35

40 ..'H........ । Tdt 50 60 70 80 #11644: Acetonitrile, dichloro- I 108 11 । 1 1 > ■ । 1 > ।1 l 1 > 90 100 110

74 3.50 3.60 3.70 3.80 3.90 35 m/z47.00 26.25%

5000 82

47

m/z~> 0 ■ i •

10 • ■ ■

20 i • ■ ■ ■ । •

30 40 50 • < i • ■ • • । > 60 70 80 1 ■

90 i ■ ■ ■ ■

100 i ■ ■ ■ ■

110 i ■ )...... A.... I.. 3.50 3.60 3.70 3.80 3.90

)0314.D SCAN508.M Tue Jan 15- 08:47:50 2002 Page 3

NYC-WTC_000051370