GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\00003A.D Vial: 2 Acq On 5 Feb 2002 3:46 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Dichloroacetonitrile $$ Ace... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 3.49 0.07 ug/L 56485 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 3 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 50 4 Dichloroacetonit rile $$ Acetonit... 109 C2HC12N 003018-12-0 38 Abundance Scan 10 (3.488 min): 00003A.D (-) m/z 74.00 100.00% 74

82 5000

47 38 3.50 3.60 3.70 3.80 3.90 0! ,1 ,1 i, ,■ .‘ ...................... Il m/z 81.90 50.13% ‘ 1 1 1 1 1 I 1 1 1 1 1 1 II ' 1 1 l‘ 1 1 ' 1 1 TIit l ■ i 1 ■ ■ ■ i ■ ■ ■ ■ i ' । n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 82

5000 3.50 3.60 3.70 3.80 3.90 47 m/z 84.00 34.32% 1> 35 m/z-> 0! 1122 10 ......... 20 30 ....... 40 hi,50.,. 60 ■ i ■ 1 1 ■ i 1 70 i TUit 80 108 'I1111 r1'1 । । । । । 90 100 110 Abundance #11644: Acetonitrile, dichloro- 74 35 ‘ 3.50 3.60 3.70 3.80 3.90 5000 82 m/z 76.00 30.05% 47

n/z-> 01 ■ i ■ ■ ■ ■ i • ■ ■ • । • 10 20 30 40 Pd 50 1 ' i 1 1 1 ■ i 1 60 70 n-1 1*1—— 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74 3.50 3.60 3.70 3.80 3.90 47.00 22.47%

5000 82 47

0 - ...... 11,... h',... 35 1 1 ' 1 ' ' I ‘ I ■...... Tiit p 109— ' .AAAMA.M m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90

00003A.D SCAN508.M Thu Feb 21 10:18:49 2002 Page 3

NYC-WTC_000004806