GCMS analysis report for sample AE01547, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB21\01547.D Vial: 3 Acq On : 21 Feb 2002 4 :52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

3.49 0.10 ug/L 41262 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 74 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 64 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 64 Abundance Scan 10 (3.487 min): 01547.D (-) m/z 74.00 100.00% 74 82 5000 47 L ‘ : I'1 ■11

niz-> 01 10 m 20 30 40 50 60 70 80 ‘T-’ Ipaaagmsonans 90 100 110 m/z 3.50 3.60 3.70 3.80 3.90 81.90 62.88% Abundance #11644: Acetonitrile, dichloro- 74 35

5000 82 M/... 3.50 3.60 3.70 3.80 3.90 47 m/z 76.00 34.61% O+ ■ i ■ ■ ‘ ’ i ■ ■ ■ ■ i ‘ + H . ■ .h-,... ■ i • • > > i > +-n~r-T-r-r-p-r-r-r-|-TT miz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74 ■ ■1 ■ ।1 ■ ■11 ■ ■ ■ ■ । ■ ■ ■ ■ ।1 • ‘ ‘ । ■1 3.50 3,60 3.70 3.80 3.90 5000 82 m/z 83.90 34.36% 47 35

miz-> 0! .... 10 20 30 l,,40.. Ju,50... 60 i , T-r' 1 ‘ i • ■ ■' । ■ ■ ■ ■ । ‘ ■ i ■ ■ ■ ■ i ‘ 70 80 90 100 110 109

Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 82 ' 3.50 3.60 3.70 3.80 3.90 ' m/z 47.00 24.78% 5000 47 35 12 0 - ... Il,.. .Ill,... ■ -i ' • ‘ ■ i ■ i ‘Ii । 108 । ' I ' ■ " I ' " 1 I“ ' ■nfz-> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90

01547.D HP022102.M Mon Feb 25 10:55:24 2002 Page 3

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