GCMS analysis results for sample AD31647, Jan 25 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN22\31647.D Vial: 3 Acq Ori : 22 Jan 2002 1:51 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\SCAN5 08. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 3.48 0.16 ug/L 47597 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 74 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 74 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 74 4 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 72 Abundance Scan 9 (3.477 min): 31647.D (-) m/z 74.00 100.00%! 74 ), ...... ............................

5000 82

47 3.50 3.60 3.70 3.80 3.90 | 39 II TBt *1***‘I***I‘I m/z 81.90 48.22% nz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile 74

5000 82 N..3.50__ 3.60 3.70 3.80 3.90 | 47 m/z 76.00 32.32%

niz-> Abundance m 10 20 30 35

40 50 _______ L ' I ‘ ‘ 60 80 , TI8 109 1 1 I ' 1 1 1 I 1 1 1 1 I 1 1 ' I ‘ 70 90 100 110 #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- 74 47 82 -4-........ 3.50 3.60 3.70 3.80 3.90 TT-p-r

5000 m/z 83.95 29.68 38

‘ I ' ' ‘ ' I ‘ I ’i’ i ■ ‘ ■ i ■ ■ ■ ■ i ' 1 TIB 1 95 102108 i । l 1 ''' 1 I ' ' 1 ' I 1 1 niz-> 10 20 30 40 50 60 70 90 100 80 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... ‘ ■ i ■ ■ ■ ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■'111''1 74 3.50 3.60 3.70 3.80 3.90 1 82 m/z 47.00 20.65% 5000 47

n/z—> 12 ''111 ■1 ■ ।11 ■11' 10 20 30 35 - 40 ---*PPP 50 60 70 80 I 90 "LiB 108 ' ' I 1 1 1 1 1 1 ' 1 1 1 ' 1 100 110 /AMMYM 3.50 3.60 3.70 3.80 3.90

31647.D SCAN508.M Thu Jan 24 13:55:39 2002 Page 3

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