GCMS results for sample AE00700, Feb 13 2002

NYC 9/11 Public Portal Document Library search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB01\00700.D Vial: 7 - Acq On : 1 Feb 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 3.48 0.16 ug/L 60555 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 74 2 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 74 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 45 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 38 Abundance Scan 9 (3.477 min): 00700.D (-) m/z 74.00 100.00% 7l4

m/z--> 5000

01

Abundance ■ i ' ■ 1 ■ i ■ 10 20 — 30 38

40 47

50 60 70 #11644: Acetonitrile, dichloro- 7l4 80 L 82

1 1 i > 1 1 ■ । 90 100 ■ i ■ 110 ] 3.50 3.60 3.70 3.80 3.90 82.00 ■ ■ i ■ ' ■ ■ i ■ ■

43.96%

7 35

5000: 82 —TIT i' ■ ■ ■ i ■' ■ ‘ । ■' ■ • i 3.50 3.60 3.70 3 80 3.90 47

m/z-> 0 ' i ' ' ■ ■ i ■ ■ ’ 1 I ■ 10 20 30 40 undpuus 50 60 • ■ i • • ■ ■ i • 70 80 90 ■’T' 100 1 1 I 1 1 1 1 i 1 1 1 1 1 1 1 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74 ■ ’ i ■ i ■' ■ ■ i ■ ■ • ■ i • ■ ■ ’ i 3.50 3.60 3.70 3.80 3.90 5000 82 47.00 25.89% 47 35

Tl/Z-> 0 1 i ' ■ ' ■ i ' 10 20 _L __________ L 1 1 1 11 1 1 1 1 11'1 ' ■ l ' ' ' ' i ' 30 40 50 60 70 80 90 "It ।............... 100 110 ' Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... AAN 7l4 3.50 3.60 3.70 3.80 3.90 82 m/z 76.00 25.19%

5000 47 35

m/z-> 0 12 ■ r-, । l . ■ 10 ..... ...... ...... III,... __________ L TUB I 20 30 40 50 1 I ' ■ ■ ' l ' 60 70 80 108 I ■ i ■ ■ ■ • i ■ ■ ■ 1 l ■ ■

90 100 110 L "II 11 1 1 1111 ■ ■ i''' ■ I 3.50 3.60 3.70 3.80 3.90

0700.D SCAN508.M Mon Feb 04 08:40:50 2002 Page 3

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