GCMS analysis results for sample AE00168, Jan 2002

NYC 9/11 Public Portal Document Library search compound Report Data File : C: \MSDCHEM\1\5973N\02JAN24\00168 . D Vial: 1 Acq On : 24 Jan 2002 2:59 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \ SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 3.48 0.10 ug/L 43334 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 83 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 53 4 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 40 Abundance Scan 9 (3.476 min): 00168.D (-) m/z 74.00 100.00% 74

n N... 82 5000

47 38 |. 3.50 3.60 3.70 3.80 3.90 0 • h ■ 1 111 p "n-’ —mmTT m/z 82.00 55.15% n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile 74

5000 82 * 3.50 3.60 3.70 3.80 3.90 47 m/z 76.00 38.36% 35 ' 1 1 1 1 ' ' 1 1 1 ' ‘ l pl l 1 ' |l 1 » i । ] i । । । j J ,i • i • * » ■ i ■ ‘ 109 • j > < miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- 74 47 82 3.50 3.60 3.70 3.80 3.90 5000 m/z 83.90 34.68% .—_ 38 ........ 1 t 95 102 108 ■ ■ । ■ ■ 1 ■ । ■ ■1 ■ । ■ i ‘ 1 1 । ■ ■ * > । 1 1 < 1 । 1 "did ' 1 I 1 'I 1‘11 I'1 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 00.n—mBTIT——T103tt1t0—7 74 82 3.50 3.60 3.70 3.80 3.90 m/z 47.00 21.70% 5000 47

m/z—> mm 10 . 20 30 35 40 50 60 70 1 TIt 80 I1 ■ i ' ■ • ■ i 1 ■ 108 90 100 1 ‘ i ■ ‘

110 _AAA 3.50 3.60 3.70 3.80 3.90

0168.D SCAN508.M Fri Jan 25 10:25:52 2002 Page 3

NYC-WTC_000050506